Bicyclo[2.2.1]heptane,7-bromo-

Base Information

• Chemical Name: Bicyclo[2.2.1]heptane,7-bromo-
• CAS No.: 13237-88-2
• Molecular Formula: C7H11 Br
• Molecular Weight: 175.068
• Hs Code.: 2903890090
• Mol file: 13237-88-2.mol

Synonyms:Norbornane,7-bromo- (7CI,8CI); 7-Bromobicyclo[2.2.1]heptane; 7-Bromonorbornane

Chemical Property of Bicyclo[2.2.1]heptane,7-bromo-

Chemical Property:

• Vapor Pressure: 1.04mmHg at 25°C
• Refractive Index: n20/D 1.518
• Boiling Point: 75 °C20 mm Hg(lit.)
• Flash Point: 62.9°C
• PSA: 0.00000
• Density: 1.38 g/mL at 20 °C(lit.)
• LogP: 2.56990

Purity/Quality:

99%, ^*data from raw suppliers

7-Bromobicyclo[2.2.1]heptane technical, ≥90% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 7-Bromobicyclo[2.2.1]heptane(7-Bromonorbornane) was used in the synthesis of methyl norbornane-7-carboxylate.

Technology Process of Bicyclo[2.2.1]heptane,7-bromo-

There total 5 articles about Bicyclo[2.2.1]heptane,7-bromo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

7-iodonorbornane (70279-05-9) → 7-bromobicyclo[2.2.1]heptane (13237-88-2)

Guidance literature:

With bromine; In dichloromethane; for 5h; Heating;

DOI:10.1021/jo00135a007

Reference yield:

7,7-dibromoborbornane (51689-30-6) + dimethyl sulfate (77-78-1) → norbornene (279-23-2) + 7-bromobicyclo[2.2.1]heptane (13237-88-2) + 7-methylnorbornane (1679-14-7) + 7,7-dimethyl-norbornane (2034-53-9) + 7-norbornylidene-7-norbornane (51689-29-3) + 7-methyl-7,7'-dinorbornyl

Guidance literature:

With lithium 4,4′-di(tert-butyl)biphenyl; tertiary butyl chloride; Mechanism; Product distribution; multistep reaction;

DOI:10.1016/S0040-4039(00)60647-0

Reference yield:

anti-C7H9Br (22365-94-2) → 7-bromobicyclo[2.2.1]heptane (13237-88-2)

Guidance literature:

With ethyl acetate; platinum; Hydrogenation;

DOI:10.1021/ja01645a005

upstream raw materials:

anti-C₇H₉Br

Bicyclo[2.2.1]heptane-7-carboperoxoic acid tert-butyl ester

7-iodonorbornane

7,7-dibromoborbornane

Downstream raw materials:

bicyclo<2.2.1>heptane-7-carboxylic acid

7-carboxybicyclo<2.2.1>heptane

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