7,8-bis(benzyloxy)-3-(4-(benzyloxy)phenyl)-1,2-methylenedioxy-dibenzofuran-4-ol

Base Information

Chemical Name:7,8-bis(benzyloxy)-3-(4-(benzyloxy)phenyl)-1,2-methylenedioxy-dibenzofuran-4-ol
CAS No.:1192737-26-0
Molecular Formula:C₄₀H₃₀O₇
Molecular Weight:622.674
Hs Code.:

Synonyms:7,8-bis(benzyloxy)-3-(4-(benzyloxy)phenyl)-1,2-methylenedioxy-dibenzofuran-4-ol

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Chemical Property of 7,8-bis(benzyloxy)-3-(4-(benzyloxy)phenyl)-1,2-methylenedioxy-dibenzofuran-4-ol

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Technology Process of 7,8-bis(benzyloxy)-3-(4-(benzyloxy)phenyl)-1,2-methylenedioxy-dibenzofuran-4-ol

There total 1 articles about 7,8-bis(benzyloxy)-3-(4-(benzyloxy)phenyl)-1,2-methylenedioxy-dibenzofuran-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1192737-25-9
7,8-bis(benzyloxy)-3-(4-(benzyloxy)phenyl)-4-(methoxymethoxy)-1,2-methylenedioxydibenzofuran

: 1192737-26-0
7,8-bis(benzyloxy)-3-(4-(benzyloxy)phenyl)-1,2-methylenedioxy-dibenzofuran-4-ol

Guidance literature:: With hydrogenchloride; methanol; In dichloromethane; at 20 ℃; for 8h; Inert atmosphere;
DOI:10.1021/ol9020833

Reference yield: 89.0%

: 1192737-26-0
7,8-bis(benzyloxy)-3-(4-(benzyloxy)phenyl)-1,2-methylenedioxy-dibenzofuran-4-ol

: 501-53-1,94274-21-2
benzyl chloroformate

: 1192737-27-1
7,8-bis(benzyloxy)-4-(benzyloxycarbonyloxy)-3-(4-(benzyloxy)phenyl)-1,2-methylenedioxydibenzofuran

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol9020833

Reference yield:

: 1192737-26-0
7,8-bis(benzyloxy)-3-(4-(benzyloxy)phenyl)-1,2-methylenedioxy-dibenzofuran-4-ol

: 1596377-54-6
1,2-(acetoxymethylenedioxy)-7,8-bis(benzyloxy)-4-(phenylacetyloxy)-3-(4-(benzyloxy)phenyl)dibenzofuran

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere

1.2: 1.5 h / -78 - 0 °C / Inert atmosphere

2.1: benzene / 5 h / 80 °C / Inert atmosphere

With n-butyllithium; In tetrahydrofuran; hexane; benzene;
DOI:10.1016/j.bmc.2014.02.058