1,2-(acetoxymethylenedioxy)-7,8-bis(benzyloxy)-4-(phenylacetyloxy)-3-(4-(benzyloxy)phenyl)dibenzofuran

Base Information

Chemical Name:1,2-(acetoxymethylenedioxy)-7,8-bis(benzyloxy)-4-(phenylacetyloxy)-3-(4-(benzyloxy)phenyl)dibenzofuran
CAS No.:1596377-54-6
Molecular Formula:C₅₀H₃₈O₁₀
Molecular Weight:798.846
Hs Code.:

Synonyms:1,2-(acetoxymethylenedioxy)-7,8-bis(benzyloxy)-4-(phenylacetyloxy)-3-(4-(benzyloxy)phenyl)dibenzofuran

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Chemical Property of 1,2-(acetoxymethylenedioxy)-7,8-bis(benzyloxy)-4-(phenylacetyloxy)-3-(4-(benzyloxy)phenyl)dibenzofuran

Chemical Property:

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Technology Process of 1,2-(acetoxymethylenedioxy)-7,8-bis(benzyloxy)-4-(phenylacetyloxy)-3-(4-(benzyloxy)phenyl)dibenzofuran

There total 3 articles about 1,2-(acetoxymethylenedioxy)-7,8-bis(benzyloxy)-4-(phenylacetyloxy)-3-(4-(benzyloxy)phenyl)dibenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1596377-53-5
7,8-bis(benzyloxy)-3-(4-(benzyloxy)phenyl)-1,2-methylenedioxy-4-(phenylacetyloxy)dibenzofuran

: 546-67-8
lead(IV) tetraacetate

: 1596377-54-6
1,2-(acetoxymethylenedioxy)-7,8-bis(benzyloxy)-4-(phenylacetyloxy)-3-(4-(benzyloxy)phenyl)dibenzofuran

Guidance literature:: In benzene; at 80 ℃; for 5h; Inert atmosphere;
DOI:10.1016/j.bmc.2014.02.058

Reference yield:

: 103-80-0
phenylacetyl chloride

: 1596377-54-6
1,2-(acetoxymethylenedioxy)-7,8-bis(benzyloxy)-4-(phenylacetyloxy)-3-(4-(benzyloxy)phenyl)dibenzofuran

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere

1.2: 1.5 h / -78 - 0 °C / Inert atmosphere

2.1: benzene / 5 h / 80 °C / Inert atmosphere

With n-butyllithium; In tetrahydrofuran; hexane; benzene;
DOI:10.1016/j.bmc.2014.02.058

Reference yield:

: 1192737-26-0
7,8-bis(benzyloxy)-3-(4-(benzyloxy)phenyl)-1,2-methylenedioxy-dibenzofuran-4-ol

: 1596377-54-6
1,2-(acetoxymethylenedioxy)-7,8-bis(benzyloxy)-4-(phenylacetyloxy)-3-(4-(benzyloxy)phenyl)dibenzofuran

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere

1.2: 1.5 h / -78 - 0 °C / Inert atmosphere

2.1: benzene / 5 h / 80 °C / Inert atmosphere

With n-butyllithium; In tetrahydrofuran; hexane; benzene;
DOI:10.1016/j.bmc.2014.02.058