C₄₅H₅₆N₄O₂₂

Base Information

Chemical Name:C₄₅H₅₆N₄O₂₂
CAS No.:132446-56-1
Molecular Formula:C₄₅H₅₆N₄O₂₂
Molecular Weight:1004.95
Hs Code.:

C<sub>45</sub>H<sub>56</sub>N<sub>4</sub>O<sub>22</sub>

Synonyms:C₄₅H₅₆N₄O₂₂

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Chemical Property of C₄₅H₅₆N₄O₂₂

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Technology Process of C₄₅H₅₆N₄O₂₂

There total 6 articles about C₄₅H₅₆N₄O₂₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 132446-55-0
C₅₀H₆₂N₄O₂₄

: 132446-56-1
C₄₅H₅₆N₄O₂₂

Guidance literature:: With pyridine; hydrazinium monoacetate; for 0.1h; Ambient temperature;
DOI:10.1016/S0040-4020(01)81477-0

Reference yield:

: 3868-03-9
1,6:2,3-dianhydro-β-D-mannopyranose

: 132446-56-1
C₄₅H₅₆N₄O₂₂

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine, N,N-dimethylaminopyridine / diethyl ether / 3 h / Ambient temperature

2: 64 percent / sodium azide, p-toluenesulphonic acid, 2,6-lutidine / dimethylformamide / 72 h / 100 °C

3: 87 percent / acetic acid, trifluoroacetic acid / 20 h / 40 °C

4: 71 percent / piperidine / tetrahydrofuran / Ambient temperature

5: 89 percent / oxalyl bromide / CHCl₃; dimethylformamide / 1.5 h / Ambient temperature

6: 44 percent / silver triflate / CH₂Cl₂ / 1 h / -30 °C / molecular sieve 10 Angstroem

7: 89 percent / hydrazine acetate, pyridine / 0.1 h / Ambient temperature

With piperidine; pyridine; 2,6-dimethylpyridine; dmap; sodium azide; Oxalyl bromide; silver trifluoromethanesulfonate; hydrazinium monoacetate; toluene-4-sulfonic acid; acetic acid; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)81477-0

Reference yield:

: 132446-50-5
1,6;2,3-di-anhydro-4-O-levulinoyl-β-D-mannopyranose

: 132446-56-1
C₄₅H₅₆N₄O₂₂

Guidance literature:: Multi-step reaction with 6 steps

1: 64 percent / sodium azide, p-toluenesulphonic acid, 2,6-lutidine / dimethylformamide / 72 h / 100 °C

2: 87 percent / acetic acid, trifluoroacetic acid / 20 h / 40 °C

3: 71 percent / piperidine / tetrahydrofuran / Ambient temperature

4: 89 percent / oxalyl bromide / CHCl₃; dimethylformamide / 1.5 h / Ambient temperature

5: 44 percent / silver triflate / CH₂Cl₂ / 1 h / -30 °C / molecular sieve 10 Angstroem

6: 89 percent / hydrazine acetate, pyridine / 0.1 h / Ambient temperature

With piperidine; pyridine; 2,6-dimethylpyridine; sodium azide; Oxalyl bromide; silver trifluoromethanesulfonate; hydrazinium monoacetate; toluene-4-sulfonic acid; acetic acid; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)81477-0