N-oxy phenyl-1 dihydro-3,4-isoquinoleine

Base Information

• Chemical Name: N-oxy phenyl-1 dihydro-3,4-isoquinoleine
• CAS No.: 86448-84-2
• Molecular Formula: C₁₅H₁₃NO
• Molecular Weight: 223.274

Synonyms:N-oxy phenyl-1 dihydro-3,4-isoquinoleine

Chemical Property of N-oxy phenyl-1 dihydro-3,4-isoquinoleine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

SDS file from LookChem

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Technology Process of N-oxy phenyl-1 dihydro-3,4-isoquinoleine

There total 4 articles about N-oxy phenyl-1 dihydro-3,4-isoquinoleine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

1-phenyl-1,2,3,4-tetrahydroisoquinoline (22990-19-8) → N-oxy phenyl-1 dihydro-3,4-isoquinoleine (86448-84-2)

Guidance literature:

With dihydrogen peroxide; In acetonitrile; at 20 ℃; for 4h; Solvent; Temperature;

DOI:10.1021/acs.joc.1c01888

Reference yield: 50.0%

1-phenyl-3,4-dihydroisoquinoline (52250-50-7) → 1-phenylisoquinoline (3297-72-1) + N-oxy phenyl-1 dihydro-3,4-isoquinoleine (86448-84-2)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 1h;

DOI:10.1016/0040-4020(82)85031-X

Reference yield: 50.0%

N-benzoyl N-hydroxy <(benzoyl-2) phenyl-2 ethylamine> (86448-88-6) → N-oxy phenyl-1 dihydro-3,4-isoquinoleine (86448-84-2)

Guidance literature:

With acide toluene-p-sulfonique; In methanol; for 2h; Heating;

DOI:10.1016/0040-4020(82)85031-X

upstream raw materials:

1-phenyl-3,4-dihydroisoquinoline

N-benzoyl N-hydroxy <(benzoyl-2) phenyl-2 ethylamine>

N-benzoyl N-benzoyloxy <(benzoyl-2) phenyl-2 ethylamine>

1-phenyl-1,2,3,4-tetrahydroisoquinoline

Downstream raw materials:

1-phenylisoquinoline

2-phenyl-3,4-dihydroisoquinolin-1(2H)-one

1-phenyl-3,4-dihydroisoquinoline

1-phenyl-1,2,3,4-tetrahydroisoquinoline

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