Technology Process of Silver decanoate
There total 2 articles about Silver decanoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
NaOH;
In
ethanol; water;
soln. of acid in EtOH was combined with NaOH in EtOH; aq. soln. of Ag salt was added dropwise with stirring at 343 K; stirred for 30 min at ambient temp.; filtered; washed (acetone/CH2Cl2, 1/1); dried in vac. for 24 h; elem. anal.;
DOI:10.1039/c2dt11638c
- Guidance literature:
-
In
water;
an aq. soln. of silver nitrate added to an aq. soln. of the fatty acid sodium salt, stirred by Teflon magnetic stirrer; precipitate filtered and washed by ethanol and dried under vacuum;
DOI:10.1246/cl.2004.158
- Guidance literature:
-
With
hexan-1-ol;
In
further solvent(s);
byproducts: CH3(CH2)4CHO; fatty acid silver salt added to 1-hexanol; the suspension stirred and heated up to 413 K under MW irradiation within 2 min under N2 atmosphere; maintained for 5 min at 413 K (or 40 min at 383 K, or 1 min at 430 K) under repeated on-off MW irradiation; suspension cooled down by an air blower;
DOI:10.1246/cl.2004.158