C₂₆H₁₇Cl₂F₂NO₅

Base Information

Chemical Name:C₂₆H₁₇Cl₂F₂NO₅
CAS No.:333447-83-9
Molecular Formula:C₂₆H₁₇Cl₂F₂NO₅
Molecular Weight:532.327
Hs Code.:

C<sub>26</sub>H<sub>17</sub>Cl<sub>2</sub>F<sub>2</sub>NO<sub>5</sub>

Synonyms:C₂₆H₁₇Cl₂F₂NO₅

Suppliers and Price of C₂₆H₁₇Cl₂F₂NO₅

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₆H₁₇Cl₂F₂NO₅

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₆H₁₇Cl₂F₂NO₅

There total 6 articles about C₂₆H₁₇Cl₂F₂NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 557-21-1
dicyanozinc

: 333447-73-7
1-(3,5-bis-O-(p-chlorobenzoyl)-2'-deoxy-β-D-ribofuranosyl)-2,4-difluoro-5-iodobenzene

: 333447-83-9
C₂₆H₁₇Cl₂F₂NO₅

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 80 - 90 ℃; for 4h;
DOI:10.1081/NCN-100001435

Reference yield:

: 348-57-2
2,4-difluorobromobenzene

: 333447-83-9
C₂₆H₁₇Cl₂F₂NO₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: Mg; I₂ / tetrahydrofuran / 1 h / 40 °C

1.2: CdCl₂ / 1 h / Heating

1.3: 7 percent / 12 h / 25 °C

2.1: 91 percent / N-iodosuccinimide / trifluoroacetic acid / 20 h / 25 °C

3.1: 94 percent / Pd(PPh₄)3 / dimethylformamide / 4 h / 80 - 90 °C

With N-iodo-succinimide; iodine; magnesium; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; N,N-dimethyl-formamide; trifluoroacetic acid;
DOI:10.1081/NCN-100001435

Reference yield:

: 122-01-0
4-chloro-benzoyl chloride

: 333447-83-9
C₂₆H₁₇Cl₂F₂NO₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: AcCl; MeOH / 0.75 h / 25 °C

1.2: pyridine; DMAP / 0 - 25 °C

1.3: 82 percent / HCl gas / diethyl ether; acetic acid / 0.17 h / 0 °C

2.1: Mg; I₂ / tetrahydrofuran / 1 h / 40 °C

2.2: CdCl₂ / 1 h / Heating

2.3: 7 percent / 12 h / 25 °C

3.1: 91 percent / N-iodosuccinimide / trifluoroacetic acid / 20 h / 25 °C

4.1: 94 percent / Pd(PPh₄)3 / dimethylformamide / 4 h / 80 - 90 °C

With methanol; N-iodo-succinimide; iodine; magnesium; acetyl chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; N,N-dimethyl-formamide; trifluoroacetic acid;
DOI:10.1081/NCN-100001435