2-(2-Chlorophenyl)-N-(3,3-difluorocyclohexyl)-2-(3-fluorophenylamino)-acetamide

Base Information

Chemical Name:2-(2-Chlorophenyl)-N-(3,3-difluorocyclohexyl)-2-(3-fluorophenylamino)-acetamide
CAS No.:1448310-16-4
Molecular Formula:C₂₀H₂₀ClF₃N₂O
Molecular Weight:396.84
Hs Code.:

Synonyms:2-(2-Chlorophenyl)-N-(3,3-difluorocyclohexyl)-2-(3-fluorophenylamino)-acetamide

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Chemical Property of 2-(2-Chlorophenyl)-N-(3,3-difluorocyclohexyl)-2-(3-fluorophenylamino)-acetamide

Chemical Property:

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Technology Process of 2-(2-Chlorophenyl)-N-(3,3-difluorocyclohexyl)-2-(3-fluorophenylamino)-acetamide

There total 4 articles about 2-(2-Chlorophenyl)-N-(3,3-difluorocyclohexyl)-2-(3-fluorophenylamino)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1103583-04-5
(3-fluoro-phenylamino)-phenyl-acetic acid

: 921602-77-9
3,3-difluorocyclohexanamine hydrochloride

: 1448310-16-4
2-(2-Chlorophenyl)-N-(3,3-difluorocyclohexyl)-2-(3-fluorophenylamino)-acetamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 921602-76-8
benzyl N-(3,3-difluorocyclohexyl)carbamate

: 1448310-16-4
2-(2-Chlorophenyl)-N-(3,3-difluorocyclohexyl)-2-(3-fluorophenylamino)-acetamide

Guidance literature:: Multi-step reaction with 2 steps

2: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / water

With N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In water;

Reference yield:

: 320590-29-2
benzyl (3-oxocyclohexyl)carbamate

: 1448310-16-4
2-(2-Chlorophenyl)-N-(3,3-difluorocyclohexyl)-2-(3-fluorophenylamino)-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: diethylamino-sulfur trifluoride; sodium hydrogencarbonate / dichloromethane

3: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / water

With diethylamino-sulfur trifluoride; sodium hydrogencarbonate; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In dichloromethane; water;