2-[1-[4-(2-Phenoxy-ethoxy)-phenyl]-meth-(Z)-ylidene]-1-aza-bicyclo[2.2.2]octan-3-one

Base Information

• Chemical Name: 2-[1-[4-(2-Phenoxy-ethoxy)-phenyl]-meth-(Z)-ylidene]-1-aza-bicyclo[2.2.2]octan-3-one
• CAS No.: 103660-33-9
• Molecular Formula: C₂₂H₂₃NO₃
• Molecular Weight: 349.43

Synonyms:2-[1-[4-(2-Phenoxy-ethoxy)-phenyl]-meth-(Z)-ylidene]-1-aza-bicyclo[2.2.2]octan-3-one

Chemical Property of 2-[1-[4-(2-Phenoxy-ethoxy)-phenyl]-meth-(Z)-ylidene]-1-aza-bicyclo[2.2.2]octan-3-one

Chemical Property:

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Technology Process of 2-[1-[4-(2-Phenoxy-ethoxy)-phenyl]-meth-(Z)-ylidene]-1-aza-bicyclo[2.2.2]octan-3-one

There total 1 articles about 2-[1-[4-(2-Phenoxy-ethoxy)-phenyl]-meth-(Z)-ylidene]-1-aza-bicyclo[2.2.2]octan-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

1-azabicyclo[2.2.1]heptan-3-one (21472-89-9) + 4-(2-phenoxyethyloxy)benzaldehyde (103660-61-3) → 2-[1-[4-(2-Phenoxy-ethoxy)-phenyl]-meth-(Z)-ylidene]-1-aza-bicyclo[2.2.2]octan-3-one (103660-33-9)

Guidance literature:

With sodium hydroxide; In ethanol; 1) 5 h, reflux, 2) 16 h, 20 deg C;

DOI:10.1007/BF00515032

Reference yield: 92.0%

2-[1-[4-(2-Phenoxy-ethoxy)-phenyl]-meth-(Z)-ylidene]-1-aza-bicyclo[2.2.2]octan-3-one (103660-33-9) → 2-<4-(β-phenoxyethoxy)benzyl>-3-oxoquinuclidine (103660-59-9)

Guidance literature:

With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; ethanol;

DOI:10.1007/BF00515032

Reference yield: 81.0%

2-[1-[4-(2-Phenoxy-ethoxy)-phenyl]-meth-(Z)-ylidene]-1-aza-bicyclo[2.2.2]octan-3-one (103660-33-9) → 4-{5-[4-(2-Phenoxy-ethoxy)-phenyl]-1H-pyrazol-3-yl}-piperidine (103660-48-6)

Guidance literature:

With potassium hydroxide; hydrazine hydrate; In ethylene glycol; at 165 - 170 ℃; for 7h;

DOI:10.1007/BF00515032

upstream raw materials:

1-azabicyclo[2.2.1]heptan-3-one

4-(2-phenoxyethyloxy)benzaldehyde

Downstream raw materials:

3-[4-(2-Phenoxy-ethoxy)-phenyl]-1,4,5-triaza-tricyclo[5.2.2.0^2,6]undecan-6-ol

2-<4-(β-phenoxyethoxy)benzyl>-3-oxoquinuclidine

4-{5-[4-(2-Phenoxy-ethoxy)-phenyl]-1H-pyrazol-3-yl}-piperidine

3-[4-(2-Phenoxy-ethoxy)-phenyl]-1,4,5-triaza-tricyclo[5.2.2.0^2,6]undec-5-ene

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