C₃₂H₃₉N₅O₄

Base Information

Chemical Name:C₃₂H₃₉N₅O₄
CAS No.:1552292-97-3
Molecular Formula:C₃₂H₃₉N₅O₄
Molecular Weight:557.693
Hs Code.:

C<sub>32</sub>H<sub>39</sub>N<sub>5</sub>O<sub>4</sub>

Synonyms:C₃₂H₃₉N₅O₄

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Chemical Property of C₃₂H₃₉N₅O₄

Chemical Property:

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Technology Process of C₃₂H₃₉N₅O₄

There total 5 articles about C₃₂H₃₉N₅O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58717-02-5
3-cyclohexyl-D-alanine

: 1552292-97-3
C₃₂H₃₉N₅O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: thionyl chloride / 18 h / -20 °C / Reflux

2.1: N-ethyl-N,N-diisopropylamine / 36 h / 20 °C / pH 9

3.1: N-ethyl-N,N-diisopropylamine / 37 h / 20 °C

4.1: sodium hydroxide; water / 1,4-dioxane / 16 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; benzotriazol-1-ol / N,N-dimethyl-formamide / 3.5 h / 20 °C

5.2: 20 °C

With thionyl chloride; water; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.12.094

Reference yield:

: C₉H₁₀N₃OPol

: 96402-49-2,138774-93-3
N^α-Fmoc-3-(1'-naphthyl)alanine

: 190904-21-3
(2R)-2-[(tert-butoxycarbonyl)(2-tert-butoxy-2-oxoethyl)amino]-3-cyclohexylpropanoic acid

: 1552292-97-3
C₃₂H₃₉N₅O₄

Guidance literature:: C₉H₁₀N₃OPol; N^α-Fmoc-3-(1'-naphthyl)alanine; With benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 3.5h; para-nitrophenyl Wang carbamate resin

With trifluoroacetic acid; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; para-nitrophenyl Wang carbamate resin

(2R)-2-[(tert-butoxycarbonyl)(2-tert-butoxy-2-oxoethyl)amino]-3-cyclohexylpropanoic acid; Further stages;
DOI:10.1016/j.bmcl.2013.12.094

Reference yield:

: 144644-00-8
methyl (R)-2-amino-3-cyclohexylpropanoate hydrochloride

: 1552292-97-3
C₃₂H₃₉N₅O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-ethyl-N,N-diisopropylamine / 36 h / 20 °C / pH 9

2.1: N-ethyl-N,N-diisopropylamine / 37 h / 20 °C

3.1: sodium hydroxide; water / 1,4-dioxane / 16 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; benzotriazol-1-ol / N,N-dimethyl-formamide / 3.5 h / 20 °C

4.2: 20 °C

With water; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.12.094