1-(5-((4-chlorophenyl)thio)-2-methyl-1,4-diphenyl-1H-pyrrol-3-yl)ethanone

Base Information

Chemical Name:1-(5-((4-chlorophenyl)thio)-2-methyl-1,4-diphenyl-1H-pyrrol-3-yl)ethanone
CAS No.:1456593-35-3
Molecular Formula:C₂₅H₂₀ClNOS
Molecular Weight:417.959
Hs Code.:

Synonyms:1-(5-((4-chlorophenyl)thio)-2-methyl-1,4-diphenyl-1H-pyrrol-3-yl)ethanone

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Chemical Property of 1-(5-((4-chlorophenyl)thio)-2-methyl-1,4-diphenyl-1H-pyrrol-3-yl)ethanone

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Technology Process of 1-(5-((4-chlorophenyl)thio)-2-methyl-1,4-diphenyl-1H-pyrrol-3-yl)ethanone

There total 4 articles about 1-(5-((4-chlorophenyl)thio)-2-methyl-1,4-diphenyl-1H-pyrrol-3-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1142-19-4
4,4'-dichlorodiphenyl disulfide

: 155014-69-0
1-(2-methyl-1,4-diphenyl-1H-pyrrol-3-yl)ethanone

: 1456593-35-3
1-(5-((4-chlorophenyl)thio)-2-methyl-1,4-diphenyl-1H-pyrrol-3-yl)ethanone

Guidance literature:: 4,4'-dichlorodiphenyl disulfide; With trichloroisocyanuric acid; In ethyl acetate; at 20 ℃;

1-(2-methyl-1,4-diphenyl-1H-pyrrol-3-yl)ethanone; In ethyl acetate; at 20 ℃; for 0.75h;
DOI:10.1016/j.tet.2013.08.035

Reference yield:

: 102-96-5
(2-nitroethenyl)benzene

: 1456593-35-3
1-(5-((4-chlorophenyl)thio)-2-methyl-1,4-diphenyl-1H-pyrrol-3-yl)ethanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: cerium(III) chloride heptahydrate / nitromethane / 0.25 h / 100 °C / Microwave irradiation

2.1: trichloroisocyanuric acid / ethyl acetate / 20 °C

2.2: 0.75 h / 20 °C

With cerium(III) chloride heptahydrate; trichloroisocyanuric acid; In nitromethane; ethyl acetate;
DOI:10.1016/j.tet.2013.08.035

Reference yield:

: 123-54-6,81235-32-7
acetylacetone

: 1456593-35-3
1-(5-((4-chlorophenyl)thio)-2-methyl-1,4-diphenyl-1H-pyrrol-3-yl)ethanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: cerium(III) chloride heptahydrate / nitromethane / 0.25 h / 100 °C / Microwave irradiation

2.1: trichloroisocyanuric acid / ethyl acetate / 20 °C

2.2: 0.75 h / 20 °C

With cerium(III) chloride heptahydrate; trichloroisocyanuric acid; In nitromethane; ethyl acetate;
DOI:10.1016/j.tet.2013.08.035