2-Propyn-1-amine,N-ethyl-N-2-propynyl-(9CI)

Base Information

• Chemical Name: 2-Propyn-1-amine,N-ethyl-N-2-propynyl-(9CI)
• CAS No.: 13002-92-1
• Molecular Formula: C8H11 N
• Molecular Weight: 121.18
• Mol file: 13002-92-1.mol

Synonyms:2-Propyn-1-amine,N-ethyl-N-2-propynyl- (9CI); Di-2-propynylamine, N-ethyl- (7CI,8CI);Ethyldipropargylamine

Chemical Property of 2-Propyn-1-amine,N-ethyl-N-2-propynyl-(9CI)

Chemical Property:

• Boiling Point: 84 - 86 °C (65 mmHg)
• PSA: 3.24000
• LogP: 0.57470

Purity/Quality:

99% ^*data from raw suppliers

N-ETHYL-N-2-PROPYNYL-2-PROPYN-1-AMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Propyn-1-amine,N-ethyl-N-2-propynyl-(9CI)

There total 2 articles about 2-Propyn-1-amine,N-ethyl-N-2-propynyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

ethylamine (75-04-7,85404-22-4) + propargyl bromide (106-96-7) → N-(ethyl)propargylamine (6943-44-8) + N-ethyl-N,N-diproparglylamine (13002-92-1)

Guidance literature:

In water; at 20 ℃;

DOI:10.1134/S1070428020010311

Reference yield:

ethylamine (75-04-7,85404-22-4) + propargyl bromide (106-96-7) → N-ethyl-N,N-diproparglylamine (13002-92-1)

Guidance literature:

With sodium hydroxide;

DOI:10.1021/jo01344a510

Reference yield: 60.0%

N-ethyl-N,N-diproparglylamine (13002-92-1) + methyl 4-(azidomethyl)benzoate (94341-53-4) → C26H29N7O4

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; water; at 50 - 60 ℃; for 7h;

DOI:10.1039/c4cc06348a

upstream raw materials:

ethylamine

propargyl bromide