3-ethoxycarbonyl-3-ethoxycarbonylmethyl-2-tosyl-5,6-benzo isoindolin-1-one

Base Information

Chemical Name:3-ethoxycarbonyl-3-ethoxycarbonylmethyl-2-tosyl-5,6-benzo isoindolin-1-one
CAS No.:1356832-67-1
Molecular Formula:C₂₆H₂₅NO₇S
Molecular Weight:495.553
Hs Code.:

Synonyms:3-ethoxycarbonyl-3-ethoxycarbonylmethyl-2-tosyl-5,6-benzo isoindolin-1-one

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Chemical Property of 3-ethoxycarbonyl-3-ethoxycarbonylmethyl-2-tosyl-5,6-benzo isoindolin-1-one

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Technology Process of 3-ethoxycarbonyl-3-ethoxycarbonylmethyl-2-tosyl-5,6-benzo isoindolin-1-one

There total 3 articles about 3-ethoxycarbonyl-3-ethoxycarbonylmethyl-2-tosyl-5,6-benzo isoindolin-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: N-tosyl-2-naphthamide

: 623-91-6
diethyl Fumarate

: 1356832-67-1
3-ethoxycarbonyl-3-ethoxycarbonylmethyl-2-tosyl-5,6-benzo isoindolin-1-one

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate; In toluene; at 130 ℃; for 48h; regioselective reaction; Inert atmosphere;
DOI:10.1039/c2cc16963k

Reference yield: 76.0%

: 623-73-4
diazoacetic acid ethyl ester

: N-tosyl-2-naphthamide

: 1356832-67-1
3-ethoxycarbonyl-3-ethoxycarbonylmethyl-2-tosyl-5,6-benzo isoindolin-1-one

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate; In toluene; at 130 ℃; for 48h; Inert atmosphere;
DOI:10.1016/j.tet.2012.08.095

Reference yield:

: 81589-31-3
N-(p-toluenesulfonyl)-1-naphthanamide

: 623-91-6
diethyl Fumarate

: 1356832-68-2
C₂₆H₂₅NO₇S

: 1356832-67-1
3-ethoxycarbonyl-3-ethoxycarbonylmethyl-2-tosyl-5,6-benzo isoindolin-1-one

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate; In toluene; at 130 ℃; for 48h; Inert atmosphere;
DOI:10.1039/c2cc16963k