N-methyl-3-nitro-4-[(3,3,3-trifluoro-1-methylpropyl)oxy]benzenesuIfonamide

Base Information

Chemical Name:N-methyl-3-nitro-4-[(3,3,3-trifluoro-1-methylpropyl)oxy]benzenesuIfonamide
CAS No.:1351094-59-1
Molecular Formula:C₁₁H₁₃F₃N₂O₅S
Molecular Weight:342.296
Hs Code.:

Synonyms:N-methyl-3-nitro-4-[(3,3,3-trifluoro-1-methylpropyl)oxy]benzenesuIfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-3-nitro-4-[(3,3,3-trifluoro-1-methylpropyl)oxy]benzenesuIfonamide

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Technology Process of N-methyl-3-nitro-4-[(3,3,3-trifluoro-1-methylpropyl)oxy]benzenesuIfonamide

There total 3 articles about N-methyl-3-nitro-4-[(3,3,3-trifluoro-1-methylpropyl)oxy]benzenesuIfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1041598-53-1
4-fluoro-N-methyl-3-nitrobenzenesulfonamide

: 101054-93-7
4,4,4-trifluoro-2-butanol

: 1351094-59-1
N-methyl-3-nitro-4-[(3,3,3-trifluoro-1-methylpropyl)oxy]benzenesuIfonamide

Guidance literature:: 4,4,4-trifluoro-2-butanol; With sodium hydride; In 1,4-dioxane; mineral oil; at 0 - 20 ℃; for 0.5h; Sealed vessel;

4-fluoro-N-methyl-3-nitrobenzenesulfonamide; In 1,4-dioxane; at 110 ℃; for 20h; Sealed vessel;

Reference yield:

: 6668-56-0
4-fluoro-3-nitrobenzene-1-sulfonyl chloride

: 1351094-59-1
N-methyl-3-nitro-4-[(3,3,3-trifluoro-1-methylpropyl)oxy]benzenesuIfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / tetrahydrofuran / 1 h / -35 °C

2.1: sodium hydride / 1,4-dioxane; mineral oil / 0.5 h / 0 - 20 °C / Sealed vessel

2.2: 20 h / 110 °C / Sealed vessel

With sodium hydride; triethylamine; In tetrahydrofuran; 1,4-dioxane; mineral oil;

Reference yield:

: 1493-27-2,127723-77-7
ortho-nitrofluorobenzene

: 1351094-59-1
N-methyl-3-nitro-4-[(3,3,3-trifluoro-1-methylpropyl)oxy]benzenesuIfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: chlorosulfonic acid / 18 h / 100 °C

2.1: triethylamine / tetrahydrofuran / 1 h / -35 °C

3.1: sodium hydride / 1,4-dioxane; mineral oil / 0.5 h / 0 - 20 °C / Sealed vessel

3.2: 20 h / 110 °C / Sealed vessel

With chlorosulfonic acid; sodium hydride; triethylamine; In tetrahydrofuran; 1,4-dioxane; mineral oil;