3-amino-N-methyl-4-[(3,3,3-trifluoro-1-methylpropyl)oxy]-1,5-cyclohexadiene-1-sulfonamide

Base Information

Chemical Name:3-amino-N-methyl-4-[(3,3,3-trifluoro-1-methylpropyl)oxy]-1,5-cyclohexadiene-1-sulfonamide
CAS No.:1351094-61-5
Molecular Formula:C₁₁H₁₅F₃N₂O₃S
Molecular Weight:312.313
Hs Code.:

Synonyms:3-amino-N-methyl-4-[(3,3,3-trifluoro-1-methylpropyl)oxy]-1,5-cyclohexadiene-1-sulfonamide

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Chemical Property of 3-amino-N-methyl-4-[(3,3,3-trifluoro-1-methylpropyl)oxy]-1,5-cyclohexadiene-1-sulfonamide

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Technology Process of 3-amino-N-methyl-4-[(3,3,3-trifluoro-1-methylpropyl)oxy]-1,5-cyclohexadiene-1-sulfonamide

There total 4 articles about 3-amino-N-methyl-4-[(3,3,3-trifluoro-1-methylpropyl)oxy]-1,5-cyclohexadiene-1-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1351094-59-1
N-methyl-3-nitro-4-[(3,3,3-trifluoro-1-methylpropyl)oxy]benzenesuIfonamide

: 1351094-61-5
3-amino-N-methyl-4-[(3,3,3-trifluoro-1-methylpropyl)oxy]-1,5-cyclohexadiene-1-sulfonamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 0.75h; under 1810.07 Torr;

Reference yield:

: 1493-27-2,127723-77-7
ortho-nitrofluorobenzene

: 1351094-61-5
3-amino-N-methyl-4-[(3,3,3-trifluoro-1-methylpropyl)oxy]-1,5-cyclohexadiene-1-sulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: chlorosulfonic acid / 18 h / 100 °C

2.1: triethylamine / tetrahydrofuran / 1 h / -35 °C

3.1: sodium hydride / 1,4-dioxane; mineral oil / 0.5 h / 0 - 20 °C / Sealed vessel

3.2: 20 h / 110 °C / Sealed vessel

4.1: hydrogen / palladium on activated charcoal / ethanol / 0.75 h / 1810.07 Torr

With chlorosulfonic acid; hydrogen; sodium hydride; triethylamine; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; ethanol; mineral oil;

Reference yield:

: 6668-56-0
4-fluoro-3-nitrobenzene-1-sulfonyl chloride

: 1351094-61-5
3-amino-N-methyl-4-[(3,3,3-trifluoro-1-methylpropyl)oxy]-1,5-cyclohexadiene-1-sulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / tetrahydrofuran / 1 h / -35 °C

2.1: sodium hydride / 1,4-dioxane; mineral oil / 0.5 h / 0 - 20 °C / Sealed vessel

2.2: 20 h / 110 °C / Sealed vessel

3.1: hydrogen / palladium on activated charcoal / ethanol / 0.75 h / 1810.07 Torr

With hydrogen; sodium hydride; triethylamine; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; ethanol; mineral oil;