5-hydroxy-4-phenylthiomethyl-exo-10-oxatricyclo<5.2.1.0^2,6>deca-4,8-dien-3-one

Base Information

• Chemical Name: 5-hydroxy-4-phenylthiomethyl-exo-10-oxatricyclo<5.2.1.0^2,6>deca-4,8-dien-3-one
• CAS No.: 127588-18-5
• Molecular Formula: C₁₆H₁₄O₃S
• Molecular Weight: 286.351

Synonyms:5-hydroxy-4-phenylthiomethyl-exo-10-oxatricyclo<5.2.1.0^2,6>deca-4,8-dien-3-one

Chemical Property of 5-hydroxy-4-phenylthiomethyl-exo-10-oxatricyclo<5.2.1.0^2,6>deca-4,8-dien-3-one

Chemical Property:

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Technology Process of 5-hydroxy-4-phenylthiomethyl-exo-10-oxatricyclo<5.2.1.0^2,6>deca-4,8-dien-3-one

There total 2 articles about 5-hydroxy-4-phenylthiomethyl-exo-10-oxatricyclo<5.2.1.0^2,6>deca-4,8-dien-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 5-hydroxy-exo-10-oxatricyclo<5.2.1.02,6>deca-4,8-dien-3-one (62926-69-6,69608-99-7) + thiophenol (108-98-5) → 5-hydroxy-4-phenylthiomethyl-exo-10-oxatricyclo<5.2.1.02,6>deca-4,8-dien-3-one (127588-18-5)

Guidance literature:

With triethylamine; In ethanol; water; at 70 ℃; for 24h; Yield given;

DOI:10.1016/S0040-4020(01)89179-1

Reference yield:

maleic anhydride (930-60-9) → 5-hydroxy-4-phenylthiomethyl-exo-10-oxatricyclo<5.2.1.02,6>deca-4,8-dien-3-one (127588-18-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / 336 h

2: triethylamine / ethanol; H₂O / 24 h / 70 °C

With triethylamine; In ethanol; water;

DOI:10.1016/S0040-4020(01)89179-1

Reference yield:

triethyloxonium fluoroborate (368-39-8) + 5-hydroxy-4-phenylthiomethyl-exo-10-oxatricyclo<5.2.1.02,6>deca-4,8-dien-3-one (127588-18-5) → Ethyl phenyl sulfide (622-38-8) + 5-ethoxy-4-phenylthiomethyl-exo-10-oxatricyclo<5.2.1.02,6>deca-4,8-dien-3-one (112698-59-6)

Guidance literature:

With triethylamine; In dichloromethane; Yield given;

DOI:10.1016/S0040-4020(01)89179-1

upstream raw materials:

formaldehyd

5-hydroxy-exo-10-oxatricyclo<5.2.1.0^2,6>deca-4,8-dien-3-one

thiophenol

maleic anhydride

Downstream raw materials:

Ethyl phenyl sulfide

5-ethoxy-4-phenylthiomethyl-exo-10-oxatricyclo<5.2.1.0^2,6>deca-4,8-dien-3-one

4-phenylthiomethyl-exo-10-oxatricyclo<5.2.1.0^2,6>deca-4,8-dien-3-one

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