4-(6-azidohexyl)-1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene iodoborane

Base Information

• Chemical Name: 4-(6-azidohexyl)-1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene iodoborane
• CAS No.: 1338728-96-3
• Molecular Formula: C₃₃H₄₉BIN₅
• Molecular Weight: 653.501

Synonyms:4-(6-azidohexyl)-1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene iodoborane

Chemical Property of 4-(6-azidohexyl)-1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene iodoborane

Chemical Property:

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Technology Process of 4-(6-azidohexyl)-1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene iodoborane

There total 4 articles about 4-(6-azidohexyl)-1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene iodoborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-azido-6-bromohexane (235095-05-3) → 4-(6-azidohexyl)-1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene iodoborane (1338728-96-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.08 h / 20 °C / Inert atmosphere

1.2: 18 h / 20 °C / Inert atmosphere

2.1: iodine / 20 °C

With n-butyllithium; iodine; In tetrahydrofuran; hexane;

DOI:10.1021/ol202516c

Reference yield:

1,3-bis(2,6-diiopropylphenyl)imidazol-2-ylidene borane (956972-12-6) → 4-(6-azidohexyl)-1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene iodoborane (1338728-96-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.08 h / 20 °C / Inert atmosphere

1.2: 18 h / 20 °C / Inert atmosphere

2.1: iodine / 20 °C

With n-butyllithium; iodine; In tetrahydrofuran; hexane;

DOI:10.1021/ol202516c

Reference yield:

4-(6-azidohexyl)-1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene borane (1338728-76-9) → 4-(6-azidohexyl)-1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene iodoborane (1338728-96-3)

Guidance literature:

With iodine; at 20 ℃;

DOI:10.1021/ol202516c

upstream raw materials:

1,3-bis(2,6-diiopropylphenyl)imidazol-2-ylidene borane

4-(6-azidohexyl)-1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene borane

1-azido-6-bromohexane

Downstream raw materials:

4-(6-aminohexyl)-1,3-bis(2,6-diisopropylphenyl)imidazolium iodide

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