1-hydroxymethyl-2,6-dimethoxy-1-(3'-trimethylsiloxybutyl)-2,5-cyclohexadiene

Base Information

Chemical Name:1-hydroxymethyl-2,6-dimethoxy-1-(3'-trimethylsiloxybutyl)-2,5-cyclohexadiene
CAS No.:108161-74-6
Molecular Formula:C₁₆H₃₀O₄Si
Molecular Weight:314.497
Hs Code.:

Synonyms:1-hydroxymethyl-2,6-dimethoxy-1-(3'-trimethylsiloxybutyl)-2,5-cyclohexadiene

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Chemical Property of 1-hydroxymethyl-2,6-dimethoxy-1-(3'-trimethylsiloxybutyl)-2,5-cyclohexadiene

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Technology Process of 1-hydroxymethyl-2,6-dimethoxy-1-(3'-trimethylsiloxybutyl)-2,5-cyclohexadiene

There total 2 articles about 1-hydroxymethyl-2,6-dimethoxy-1-(3'-trimethylsiloxybutyl)-2,5-cyclohexadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 80900-45-4
methyl 2,6-dimethoxy-1-(3'-trimethylsilyloxybutyl)-2,5-cyclohexadiene-1-carboxylate

: 108161-74-6
1-hydroxymethyl-2,6-dimethoxy-1-(3'-trimethylsiloxybutyl)-2,5-cyclohexadiene

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 0.25h; Ambient temperature;
DOI:10.1016/S0040-4020(01)90577-0

Reference yield:

: 80900-43-2
(3-Iodo-1-methylpropoxy)trimethylsilane

: 108161-74-6
1-hydroxymethyl-2,6-dimethoxy-1-(3'-trimethylsiloxybutyl)-2,5-cyclohexadiene

Guidance literature:: Multi-step reaction with 2 steps

2: 97 percent / LiAlH₄ / diethyl ether / 0.25 h / Ambient temperature

With lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1016/S0040-4020(01)90577-0

Reference yield:

: 108161-74-6
1-hydroxymethyl-2,6-dimethoxy-1-(3'-trimethylsiloxybutyl)-2,5-cyclohexadiene

: 80900-53-4
2,6-dimethoxy-1-(methoxymethyloxymethyl)-1-(3'-oxobutyl)-2,5-cyclohexadiene

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / ethyldiisopropylamine / CH₂Cl₂ / 24 h / Ambient temperature

2: 98 percent / KF, pH 6.8 buffer / methanol / 17 h / Ambient temperature

3: 59 percent / trifluoroacetic acid, pyridine, dicyclohexylcarboximide (DCC) / dimethylsulfoxide; benzene / 24 h / Ambient temperature

With pyridine; potassium fluoride; pH 6.8 buffer; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In methanol; dichloromethane; dimethyl sulfoxide; benzene;
DOI:10.1016/S0040-4020(01)90577-0