7-phenyl-4-methyl-1,5,8-triphenyl-2,3,4-triazabicyclo<3.3.0>octa-2,7-dien-6-one

Base Information

• Chemical Name: 7-phenyl-4-methyl-1,5,8-triphenyl-2,3,4-triazabicyclo<3.3.0>octa-2,7-dien-6-one
• CAS No.: 101032-80-8
• Molecular Formula: C₃₀H₂₃N₃O
• Molecular Weight: 441.532

Synonyms:7-phenyl-4-methyl-1,5,8-triphenyl-2,3,4-triazabicyclo<3.3.0>octa-2,7-dien-6-one

Chemical Property of 7-phenyl-4-methyl-1,5,8-triphenyl-2,3,4-triazabicyclo<3.3.0>octa-2,7-dien-6-one

Chemical Property:

Purity/Quality:

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Technology Process of 7-phenyl-4-methyl-1,5,8-triphenyl-2,3,4-triazabicyclo<3.3.0>octa-2,7-dien-6-one

There total 2 articles about 7-phenyl-4-methyl-1,5,8-triphenyl-2,3,4-triazabicyclo<3.3.0>octa-2,7-dien-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

7-phenyl-1,5,8-triphenyl-2,3,4-triazabicyclo<3.3.0>octa-2,7-dien-6-one (101032-75-1) + methyl iodide (74-88-4) → 7-phenyl-4-methyl-1,5,8-triphenyl-2,3,4-triazabicyclo<3.3.0>octa-2,7-dien-6-one (101032-80-8)

Guidance literature:

With potassium tert-butylate; In dimethyl sulfoxide; benzene; for 0.75h;

DOI:10.1021/jo00359a031

Reference yield:

2,3,4,5-tetraphenylcyclopenta-2,4-dienone (479-33-4) → 7-phenyl-4-methyl-1,5,8-triphenyl-2,3,4-triazabicyclo<3.3.0>octa-2,7-dien-6-one (101032-80-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / NaN₃, conc. H₂SO₄ / dimethylformamide / 0.42 h / 20 - 80 °C

2: 35 percent / t-BuOK / dimethylsulfoxide; benzene / 0.75 h

With sodium azide; sulfuric acid; potassium tert-butylate; In dimethyl sulfoxide; N,N-dimethyl-formamide; benzene;

DOI:10.1021/jo00359a031

Reference yield: 80.0%

7-phenyl-4-methyl-1,5,8-triphenyl-2,3,4-triazabicyclo<3.3.0>octa-2,7-dien-6-one (101032-80-8) → 1-methyl-3,4,5,6-tetraphenyl-2(1H)-pyridinone (62557-82-8)

Guidance literature:

With hydrogenchloride; In methanol; for 1h; Heating;

DOI:10.1021/jo00359a031

upstream raw materials:

7-phenyl-1,5,8-triphenyl-2,3,4-triazabicyclo<3.3.0>octa-2,7-dien-6-one

methyl iodide

2,3,4,5-tetraphenylcyclopenta-2,4-dienone

Downstream raw materials:

1-methyl-3,4,5,6-tetraphenyl-2(1H)-pyridinone

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