2-(4-Chloro-benzylsulfanyl)-5-(2-methyl-[1,3]dioxolan-2-ylmethyl)-[1,3,4]oxadiazole

Base Information

• Chemical Name: 2-(4-Chloro-benzylsulfanyl)-5-(2-methyl-[1,3]dioxolan-2-ylmethyl)-[1,3,4]oxadiazole
• CAS No.: 83609-44-3
• Molecular Formula: C₁₄H₁₅ClN₂O₃S
• Molecular Weight: 326.804

Synonyms:2-(4-Chloro-benzylsulfanyl)-5-(2-methyl-[1,3]dioxolan-2-ylmethyl)-[1,3,4]oxadiazole

Chemical Property of 2-(4-Chloro-benzylsulfanyl)-5-(2-methyl-[1,3]dioxolan-2-ylmethyl)-[1,3,4]oxadiazole

Chemical Property:

Purity/Quality:

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Technology Process of 2-(4-Chloro-benzylsulfanyl)-5-(2-methyl-[1,3]dioxolan-2-ylmethyl)-[1,3,4]oxadiazole

There total 3 articles about 2-(4-Chloro-benzylsulfanyl)-5-(2-methyl-[1,3]dioxolan-2-ylmethyl)-[1,3,4]oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

fructone (6413-10-1) → 2-(4-Chloro-benzylsulfanyl)-5-(2-methyl-[1,3]dioxolan-2-ylmethyl)-[1,3,4]oxadiazole (83609-44-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 99 percent / 80percent N₂H₄*H₂O / 4 h / 100 °C

2: 78 percent / KOH / ethanol; H₂O / 2 h / Heating

3: 1.) Na, EtOH / 2.) EtOH, overnight

With potassium hydroxide; ethanol; sodium; hydrazine hydrate; In ethanol; water;

DOI:10.1007/BF00809020

Reference yield:

2-(2-methyl-1,3-dioxolan-2-yl)acetohydrazide (74949-65-8) → 2-(4-Chloro-benzylsulfanyl)-5-(2-methyl-[1,3]dioxolan-2-ylmethyl)-[1,3,4]oxadiazole (83609-44-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / KOH / ethanol; H₂O / 2 h / Heating

2: 1.) Na, EtOH / 2.) EtOH, overnight

With potassium hydroxide; ethanol; sodium; In ethanol; water;

DOI:10.1007/BF00809020

Reference yield:

1-Chloro-4-(chloromethyl)benzene (104-83-6) + 2-(2,2-Ethylendioxypropyl)-5-thiolo-1,3,4-oxadiazol (83553-11-1) → 2-(4-Chloro-benzylsulfanyl)-5-(2-methyl-[1,3]dioxolan-2-ylmethyl)-[1,3,4]oxadiazole (83609-44-3)

Guidance literature:

With ethanol; sodium; Yield given. Multistep reaction; 2.) EtOH, overnight;

DOI:10.1007/BF00809020

upstream raw materials:

1-Chloro-4-(chloromethyl)benzene

2-(2,2-Ethylendioxypropyl)-5-thiolo-1,3,4-oxadiazol

fructone

2-(2-methyl-1,3-dioxolan-2-yl)acetohydrazide

Downstream raw materials:

(Z)-1-[5-(4-Chloro-benzylsulfanyl)-[1,3,4]oxadiazol-2-yl]-propen-2-ol

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