6,3',4',2'',5'',3''',4'''-hepta-O-benzyl-1,3,2',2''',6'''-pentadeamino-1,3,2',2''',6'''-pentaazidoparomomycin

Base Information

Chemical Name:6,3',4',2'',5'',3''',4'''-hepta-O-benzyl-1,3,2',2''',6'''-pentadeamino-1,3,2',2''',6'''-pentaazidoparomomycin
CAS No.:927812-19-9
Molecular Formula:C₇₂H₇₇N₁₅O₁₄
Molecular Weight:1376.5
Hs Code.:

Synonyms:6,3',4',2'',5'',3''',4'''-hepta-O-benzyl-1,3,2',2''',6'''-pentadeamino-1,3,2',2''',6'''-pentaazidoparomomycin

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Chemical Property of 6,3',4',2'',5'',3''',4'''-hepta-O-benzyl-1,3,2',2''',6'''-pentadeamino-1,3,2',2''',6'''-pentaazidoparomomycin

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Technology Process of 6,3',4',2'',5'',3''',4'''-hepta-O-benzyl-1,3,2',2''',6'''-pentadeamino-1,3,2',2''',6'''-pentaazidoparomomycin

There total 2 articles about 6,3',4',2'',5'',3''',4'''-hepta-O-benzyl-1,3,2',2''',6'''-pentadeamino-1,3,2',2''',6'''-pentaazidoparomomycin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1073243-50-1
1,3,2',2',6'-pentaazido-6,3',2,5,3',4'-hexa-O-benzyl-4',6'-O-benzylidene-1,3,2',2',6'-pentadeaminoparomomycin

: 927812-19-9
6,3',4',2'',5'',3''',4'''-hepta-O-benzyl-1,3,2',2''',6'''-pentadeamino-1,3,2',2''',6'''-pentaazidoparomomycin

Guidance literature:: With dimethylsulfide borane complex; di-n-butylboryl trifluoromethanesulfonate; In dichloromethane; at 0 - 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/jacs.7b07754

Reference yield: 83.0%

: 927811-93-6
perbenzylated 6'-O-Tips-perazidoparomomycin

: 927812-19-9
6,3',4',2'',5'',3''',4'''-hepta-O-benzyl-1,3,2',2''',6'''-pentadeamino-1,3,2',2''',6'''-pentaazidoparomomycin

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃;

Reference yield: 68.0%

: 927812-19-9
6,3',4',2'',5'',3''',4'''-hepta-O-benzyl-1,3,2',2''',6'''-pentadeamino-1,3,2',2''',6'''-pentaazidoparomomycin

: 6,3',4',2'',5'',3''',4'''-hepta-O-benzyl-1,3,2',2''',6'''-pentadeamino-1,3,2',2''',6'''-pentaazidoparomomycin-6'-carboxylic acid

Guidance literature:: With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide; In acetone; at 0 - 20 ℃; for 19h;
DOI:10.1021/jacs.7b07754