Technology Process of 4-nitrophenyl ((3aR,3bR,4R,7aS,8aS)-octahydro-5H-furo-[3′,2′:4,5]furo[2,3-c]pyran-4-yl)carbonate
There total 4 articles about 4-nitrophenyl ((3aR,3bR,4R,7aS,8aS)-octahydro-5H-furo-[3′,2′:4,5]furo[2,3-c]pyran-4-yl)carbonate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
at 0 - 20 ℃;
for 3h;
Inert atmosphere;
DOI:10.1021/jm400768f
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lipase amano PS-30 / tetrahydrofuran / 20 h / 23 °C / Inert atmosphere
2: pyridine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere
With
pyridine; lipase amano PS-30;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/jm400768f
- Guidance literature:
-
Multi-step reaction with 4 steps
1: palladium 10% on activated carbon; hydrogen / methanol / 12 h / 760.05 Torr / Inert atmosphere
2: L-Selectride / tetrahydrofuran / 2 h / -78 °C / Inert atmosphere
3: lipase amano PS-30 / tetrahydrofuran / 20 h / 23 °C / Inert atmosphere
4: pyridine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere
With
pyridine; palladium 10% on activated carbon; lipase amano PS-30; hydrogen; L-Selectride;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm400768f
