2'-benzenesulfonyl-5'-O-(tert-butyldimethylsilyl)-2',3'-didehydro-2',3'-dideoxyuridine

Base Information

Chemical Name:2'-benzenesulfonyl-5'-O-(tert-butyldimethylsilyl)-2',3'-didehydro-2',3'-dideoxyuridine
CAS No.:475571-76-7
Molecular Formula:C₂₁H₂₈N₂O₆SSi
Molecular Weight:464.615
Hs Code.:

Synonyms:2'-benzenesulfonyl-5'-O-(tert-butyldimethylsilyl)-2',3'-didehydro-2',3'-dideoxyuridine

Suppliers and Price of 2'-benzenesulfonyl-5'-O-(tert-butyldimethylsilyl)-2',3'-didehydro-2',3'-dideoxyuridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2'-benzenesulfonyl-5'-O-(tert-butyldimethylsilyl)-2',3'-didehydro-2',3'-dideoxyuridine

Chemical Property:

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Technology Process of 2'-benzenesulfonyl-5'-O-(tert-butyldimethylsilyl)-2',3'-didehydro-2',3'-dideoxyuridine

There total 4 articles about 2'-benzenesulfonyl-5'-O-(tert-butyldimethylsilyl)-2',3'-didehydro-2',3'-dideoxyuridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 475571-76-7
2'-benzenesulfonyl-5'-O-(tert-butyldimethylsilyl)-2',3'-didehydro-2',3'-dideoxyuridine

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / pyridine / 15 h / 20 °C

2: 80 percent / pyridine / 12 h / 20 °C

3: 100 percent / DBN / acetonitrile / 2 h / Heating

4: 79 percent / m-CPBA / methanol / 3 h / 20 °C

With pyridine; 2,6-dichloro-benzonitrile; 3-chloro-benzenecarboperoxoic acid; In methanol; acetonitrile;
DOI:10.1081/NCN-120006826

Reference yield:

: 83087-95-0
2'-deoxy-2'-phenylthiouridine

: 475571-76-7
2'-benzenesulfonyl-5'-O-(tert-butyldimethylsilyl)-2',3'-didehydro-2',3'-dideoxyuridine

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / pyridine / 15 h / 20 °C

2: 80 percent / pyridine / 12 h / 20 °C

3: 100 percent / DBN / acetonitrile / 2 h / Heating

4: 79 percent / m-CPBA / methanol / 3 h / 20 °C

With pyridine; 2,6-dichloro-benzonitrile; 3-chloro-benzenecarboperoxoic acid; In methanol; acetonitrile;
DOI:10.1081/NCN-120006826

Reference yield:

: 475571-78-9
5'-O-(tert-butyldimethylsilyl)-2'-deoxy-2'-phenylthiouridine

: 475571-76-7
2'-benzenesulfonyl-5'-O-(tert-butyldimethylsilyl)-2',3'-didehydro-2',3'-dideoxyuridine

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / pyridine / 12 h / 20 °C

2: 100 percent / DBN / acetonitrile / 2 h / Heating

3: 79 percent / m-CPBA / methanol / 3 h / 20 °C

With pyridine; 2,6-dichloro-benzonitrile; 3-chloro-benzenecarboperoxoic acid; In methanol; acetonitrile;
DOI:10.1081/NCN-120006826