dimethyl rac-2-{[bis(benzyloxy)phosphoryl]methyl}-4-fluoropentanedioate

Base Information

Chemical Name:dimethyl rac-2-{[bis(benzyloxy)phosphoryl]methyl}-4-fluoropentanedioate
CAS No.:1312438-54-2
Molecular Formula:C₂₂H₂₆FO₇P
Molecular Weight:452.416
Hs Code.:

Synonyms:dimethyl rac-2-{[bis(benzyloxy)phosphoryl]methyl}-4-fluoropentanedioate

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Chemical Property of dimethyl rac-2-{[bis(benzyloxy)phosphoryl]methyl}-4-fluoropentanedioate

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Technology Process of dimethyl rac-2-{[bis(benzyloxy)phosphoryl]methyl}-4-fluoropentanedioate

There total 3 articles about dimethyl rac-2-{[bis(benzyloxy)phosphoryl]methyl}-4-fluoropentanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 17176-77-1
Dibenzyl phosphite

: 1312438-92-8
2-fluoro-4-methylenepentanedioic acid dimethyl ester

: 1312438-54-2
dimethyl rac-2-{[bis(benzyloxy)phosphoryl]methyl}-4-fluoropentanedioate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 4h; Microwave irradiation;

Reference yield:

: 4224-69-5
methyl 2-(bromomethyl)propenoate

: 1312438-54-2
dimethyl rac-2-{[bis(benzyloxy)phosphoryl]methyl}-4-fluoropentanedioate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; indium / water; methanol / 4 h / 5 - 35 °C

2: Nonafluorobutanesulfonyl fluoride; triethylamine; triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 20 h / 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 4 h / 50 °C / Microwave irradiation

With hydrogenchloride; indium; Nonafluorobutanesulfonyl fluoride; potassium carbonate; triethylamine tris(hydrogen fluoride); triethylamine; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;

Reference yield:

: 1312438-70-2
dimethyl 2-hydroxy-4-methylenepentanedioate

: 1312438-54-2
dimethyl rac-2-{[bis(benzyloxy)phosphoryl]methyl}-4-fluoropentanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: Nonafluorobutanesulfonyl fluoride; triethylamine; triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 20 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 50 °C / Microwave irradiation

With Nonafluorobutanesulfonyl fluoride; potassium carbonate; triethylamine tris(hydrogen fluoride); triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;