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[(R)-menthyl]2PCH2SnMe3

Base Information
  • Chemical Name:[(R)-menthyl]2PCH2SnMe3
  • CAS No.:235422-42-1
  • Molecular Formula:C24H49PSn
  • Molecular Weight:487.337
  • Hs Code.:
[(R)-menthyl]2PCH<sub>2</sub>SnMe<sub>3</sub>

Synonyms:[(R)-menthyl]2PCH2SnMe3

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Chemical Property of [(R)-menthyl]2PCH2SnMe3
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Technology Process of [(R)-menthyl]2PCH2SnMe3

There total 1 articles about [(R)-menthyl]2PCH2SnMe3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With n-BuLi; In hexane; toluene; (argon); addn. of n-BuLi in hexane at -55°C to Ph3SnCH2I in toluene, stirring (30 min), addn. of the org. P compound in toluene, warmingslowly to room temp.; addn. of water, phase sepn., washing (water), drying (Na2SO4), filtration, evapn. (vac.), extn. (pentane), concn., storage (-25°C, 18 h),sepn. of crystals, washing (pentane, -40°C), drying, recrystn. ( acetone, -25°C); elem. anal.;
Guidance literature:
With methyllithium; In diethyl ether; at -60 - 20 ℃;
Guidance literature:
With methyllithium; In diethyl ether; at -60 - 20 ℃;
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