N-[3-(7-Propyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-7-yl)-propyl]-benzamide

Base Information

Chemical Name:N-[3-(7-Propyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-7-yl)-propyl]-benzamide
CAS No.:125426-04-2
Molecular Formula:C₂₂H₂₇NO₃
Molecular Weight:353.461
Hs Code.:

Synonyms:N-[3-(7-Propyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-7-yl)-propyl]-benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[3-(7-Propyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-7-yl)-propyl]-benzamide

Chemical Property:

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Technology Process of N-[3-(7-Propyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-7-yl)-propyl]-benzamide

There total 7 articles about N-[3-(7-Propyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-7-yl)-propyl]-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 125426-03-1
3-(7-Propyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-7-yl)-propylamine

: 98-88-4
benzoyl chloride

: 125426-04-2
N-[3-(7-Propyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-7-yl)-propyl]-benzamide

Guidance literature:: With triethylamine; In dichloromethane; 0 deg C to r.t.;
DOI:10.1016/S0040-4039(00)99349-3

Reference yield:

: 67461-24-9
3-methoxy-1,5-dihydro-3H-2,4-benzodioxepine

: 125426-04-2
N-[3-(7-Propyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-7-yl)-propyl]-benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / p-toluenesulfonic acid / 1,2-dimethoxy-ethane / 0.5 h / Ambient temperature

2: 91 percent / NaN₃ / dimethylsulfoxide / Ambient temperature

3: 99 percent / LiALH₄ / diethyl ether / 0 deg C to r.t.

4: 100 percent / Et₃N / CH₂Cl₂ / 0 deg C to r.t.

With lithium aluminium tetrahydride; sodium azide; toluene-4-sulfonic acid; triethylamine; In 1,2-dimethoxyethane; diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1016/S0040-4039(00)99349-3

Reference yield:

: 84-66-2
Diethyl phthalate

: 125426-04-2
N-[3-(7-Propyl-5,9-dihydro-6,8-dioxa-benzocyclohepten-7-yl)-propyl]-benzamide

Guidance literature:: Multi-step reaction with 6 steps

1: LiAlH₄ / diethyl ether / Ambient temperature

2: 86 percent / p-toluenesulfonic acid / 1,2-dimethoxy-ethane / 0.5 h / Ambient temperature

3: 70 percent / p-toluenesulfonic acid / 1,2-dimethoxy-ethane / 0.5 h / Ambient temperature

4: 91 percent / NaN₃ / dimethylsulfoxide / Ambient temperature

5: 99 percent / LiALH₄ / diethyl ether / 0 deg C to r.t.

6: 100 percent / Et₃N / CH₂Cl₂ / 0 deg C to r.t.

With lithium aluminium tetrahydride; sodium azide; toluene-4-sulfonic acid; triethylamine; In 1,2-dimethoxyethane; diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1016/S0040-4039(00)99349-3