N-(phenylmethyl)-2-pyridinecarboselenoamide

Base Information

Chemical Name:N-(phenylmethyl)-2-pyridinecarboselenoamide
CAS No.:1608479-12-4
Molecular Formula:C₁₃H₁₂N₂Se
Molecular Weight:275.212
Hs Code.:

Synonyms:N-(phenylmethyl)-2-pyridinecarboselenoamide

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Chemical Property of N-(phenylmethyl)-2-pyridinecarboselenoamide

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Technology Process of N-(phenylmethyl)-2-pyridinecarboselenoamide

There total 1 articles about N-(phenylmethyl)-2-pyridinecarboselenoamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 18904-38-6
N-benzyl-2-pyridinecarboxamide

: 1608479-12-4
N-(phenylmethyl)-2-pyridinecarboselenoamide

Guidance literature:: With woollins’ reagent; In toluene; at 130 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo500499g

Reference yield: 61.0%

: 1608479-12-4
N-(phenylmethyl)-2-pyridinecarboselenoamide

: N,N-diphenylmethaneselenoamide

: 4,5-dihydro-2-(2-pyridyl)-N,N,4-triphenyl-5-selenazolamine

Guidance literature:: N-(phenylmethyl)-2-pyridinecarboselenoamide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 0.166667h; Inert atmosphere;

N,N-diphenylmethaneselenoamide; In tetrahydrofuran; hexane; at 0 ℃; for 1h; Inert atmosphere;

With iodine; In tetrahydrofuran; hexane; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo500499g

Reference yield:

: 1608479-12-4
N-(phenylmethyl)-2-pyridinecarboselenoamide

: 1608479-09-9
2-(2-pyridyl)-N,N,4-triphenyl-5-selenazolamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / 0 °C / Inert atmosphere

1.2: 1 h / 0 °C / Inert atmosphere

1.3: 2 h / 0 °C / Inert atmosphere

2.1: iodine / tetrahydrofuran / 18.5 h / 20 °C / Inert atmosphere

With n-butyllithium; iodine; In tetrahydrofuran; hexane;
DOI:10.1021/jo500499g