C₃₁H₃₆O₃S₂

Base Information

• Chemical Name: C₃₁H₃₆O₃S₂
• CAS No.: 1443230-62-3
• Molecular Formula: C₃₁H₃₆O₃S₂
• Molecular Weight: 520.757
• Mol file: 1443230-62-3.mol

Synonyms:C₃₁H₃₆O₃S₂

Chemical Property of C₃₁H₃₆O₃S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₁H₃₆O₃S₂

There total 1 articles about C₃₁H₃₆O₃S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

C31H36O4S2 (1443230-60-1) → C31H36O3S2 (1443230-62-3)

Guidance literature:

C₃₁H₃₆O₄S₂; With potassium selenocyanate; In water; tert-butyl alcohol; for 4h; Reflux;

With tert-butyl methyl ether; In water; tert-butyl alcohol;

DOI:10.1002/ejoc.201201184

Reference yield: 51.0%

1-tetradecene (1120-36-1) + C31H36O3S2 (1443230-62-3) → C43H60O3S2 (1443230-61-2)

Guidance literature:

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; for 4h; Inert atmosphere; Heating;

DOI:10.1002/ejoc.201201184

Reference yield:

C31H36O3S2 (1443230-62-3) → (3S,5R)-1-(4-hydroxyphenyl)nonadecane-3,5-diol (1443256-45-8)

Guidance literature:

Multi-step reaction with 3 steps

1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 4 h / Inert atmosphere; Heating

2: hydrogen / ethanol / 48 h

3: sodium hydride; ethanethiol / mineral oil; N,N-dimethyl-formamide / 10 h / Inert atmosphere; Reflux; Cooling with ice

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; hydrogen; sodium hydride; ethanethiol; In ethanol; dichloromethane; N,N-dimethyl-formamide; mineral oil; 1: |Cross Metathesis;

DOI:10.1002/ejoc.201201184

upstream raw materials:

C₃₁H₃₆O₄S₂

Downstream raw materials:

(3S,5R)-1-(4-methoxyphenyl)nonadecane-3,5-diol

(3S,5R)-1-(4-hydroxyphenyl)nonadecane-3,5-diol

C₄₃H₆₀O₃S₂