propargyl 3,5-di-O-benzyl-2-O<(S-methylthio)thiocarbonyl>-α-D-xylofuranoside

Base Information

Chemical Name:propargyl 3,5-di-O-benzyl-2-O<(S-methylthio)thiocarbonyl>-α-D-xylofuranoside
CAS No.:141357-08-6
Molecular Formula:C₂₄H₂₆O₅S₂
Molecular Weight:458.599
Hs Code.:

Synonyms:propargyl 3,5-di-O-benzyl-2-O<(S-methylthio)thiocarbonyl>-α-D-xylofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of propargyl 3,5-di-O-benzyl-2-O<(S-methylthio)thiocarbonyl>-α-D-xylofuranoside

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Technology Process of propargyl 3,5-di-O-benzyl-2-O<(S-methylthio)thiocarbonyl>-α-D-xylofuranoside

There total 1 articles about propargyl 3,5-di-O-benzyl-2-O<(S-methylthio)thiocarbonyl>-α-D-xylofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 141379-61-5
propargyl 3,5-di-O-benzyl-α-D-xylofuranoside

: 74-88-4
methyl iodide

: 141357-08-6
propargyl 3,5-di-O-benzyl-2-O<(S-methylthio)thiocarbonyl>-α-D-xylofuranoside

Guidance literature:: Yield given. Multistep reaction;
DOI:10.1016/0008-6215(92)84064-Y

Reference yield: 87.0%

: 141357-08-6
propargyl 3,5-di-O-benzyl-2-O<(S-methylthio)thiocarbonyl>-α-D-xylofuranoside

: 141357-06-4
(1S,3R,4R,5R)-4-benzyloxy-3-benzyloxymethyl-6-methylene-2,8-dioxabicyclo<3.3.0>octane

Guidance literature:: With azobisisobutyronitrile; tri-n-butyl-tin hydride; In benzene; for 1h; Heating;
DOI:10.1016/0008-6215(92)84064-Y

Reference yield:

: 141357-08-6
propargyl 3,5-di-O-benzyl-2-O<(S-methylthio)thiocarbonyl>-α-D-xylofuranoside

: 141357-10-0
(1S,3R,4R,5S,2'R)-4-benzyloxy-3-benzyloxymethyl-2,8-dioxabicyclo<3.3.0>octane-6-spiro-2'-oxirane

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / Bu3SnH, α,α'-azobisisobutyronitrile / benzene / 1 h / Heating

2: 74 percent / 3-chloroperbenzoic acid / CH₂Cl₂ / 2 h / Ambient temperature

With azobisisobutyronitrile; tri-n-butyl-tin hydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; benzene;
DOI:10.1016/0008-6215(92)84064-Y