(S)-methyl 2-(2-azidoacetamido)-3-(4-(2-fluoroethoxy)phenyl)propanoate

Base Information

Chemical Name:(S)-methyl 2-(2-azidoacetamido)-3-(4-(2-fluoroethoxy)phenyl)propanoate
CAS No.:1071476-45-3
Molecular Formula:C₁₄H₁₇FN₄O₄
Molecular Weight:324.312
Hs Code.:

Synonyms:(S)-methyl 2-(2-azidoacetamido)-3-(4-(2-fluoroethoxy)phenyl)propanoate

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Chemical Property of (S)-methyl 2-(2-azidoacetamido)-3-(4-(2-fluoroethoxy)phenyl)propanoate

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Technology Process of (S)-methyl 2-(2-azidoacetamido)-3-(4-(2-fluoroethoxy)phenyl)propanoate

There total 1 articles about (S)-methyl 2-(2-azidoacetamido)-3-(4-(2-fluoroethoxy)phenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 18523-48-3
2-azidoacetic acid

: 1071475-52-9
C₁₂H₁₆FNO₃*ClH

: 1071476-45-3
(S)-methyl 2-(2-azidoacetamido)-3-(4-(2-fluoroethoxy)phenyl)propanoate

Guidance literature:: 2-azidoacetic acid; With sodium hydrogencarbonate; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

C₁₂H₁₆FNO₃*ClH; In N,N-dimethyl-formamide; for 12h;

Reference yield:

: 1071474-90-2
6-(prop-2-ynyloxy)benzo[d]thiazole-2-sulfonamide

: 1071476-45-3
(S)-methyl 2-(2-azidoacetamido)-3-(4-(2-fluoroethoxy)phenyl)propanoate

: C₂₄H₂₅FN₆O₇S₂

Guidance literature:: With copper(II) sulfate; sodium L-ascorbate; In tetrahydrofuran; water; tert-butyl alcohol; for 12h;

Reference yield:

: 1071474-90-2
6-(prop-2-ynyloxy)benzo[d]thiazole-2-sulfonamide

: 1071476-45-3
(S)-methyl 2-(2-azidoacetamido)-3-(4-(2-fluoroethoxy)phenyl)propanoate

: 1071471-15-2
(S)-3-(4-(2-fluoroethoxy)phenyl)-2-(2-(4-((2-sulfamoylbenzo[d]thiazol-6-yloxy)methyl)-1H-1,2,3-triazol-1-yl)acetamido)propanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: copper(II) sulfate; sodium L-ascorbate / tetrahydrofuran; water; tert-butyl alcohol / 12 h

2: lithium hydroxide; water / tetrahydrofuran; tert-butyl alcohol / 2 h / 20 °C

With lithium hydroxide; water; copper(II) sulfate; sodium L-ascorbate; In tetrahydrofuran; water; tert-butyl alcohol;