1-(2-bromo-5-methylbenzyl)-5-methyl-4-(trimethylsilyl)-1H-1,2,3-triazole

Base Information

Chemical Name:1-(2-bromo-5-methylbenzyl)-5-methyl-4-(trimethylsilyl)-1H-1,2,3-triazole
CAS No.:1420532-43-9
Molecular Formula:C₁₄H₂₀BrN₃Si
Molecular Weight:338.322
Hs Code.:

Synonyms:1-(2-bromo-5-methylbenzyl)-5-methyl-4-(trimethylsilyl)-1H-1,2,3-triazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2-bromo-5-methylbenzyl)-5-methyl-4-(trimethylsilyl)-1H-1,2,3-triazole

Chemical Property:

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Technology Process of 1-(2-bromo-5-methylbenzyl)-5-methyl-4-(trimethylsilyl)-1H-1,2,3-triazole

There total 4 articles about 1-(2-bromo-5-methylbenzyl)-5-methyl-4-(trimethylsilyl)-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 6224-91-5
trimethyl(prop-1-ynyl)silane

: 1420532-42-8
2-(azidomethyl)-1-bromo-4-methyl benzene

: 1420532-43-9
1-(2-bromo-5-methylbenzyl)-5-methyl-4-(trimethylsilyl)-1H-1,2,3-triazole

Guidance literature:: In 1,2-dichloro-benzene; at 150 ℃;

Reference yield:

: 27561-50-8
1-bromo-2-(bromomethyl)-4-methylbenzene

: 1420532-43-9
1-(2-bromo-5-methylbenzyl)-5-methyl-4-(trimethylsilyl)-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / d₇-N,N-dimethylformamide / 80 °C

2: 1,2-dichloro-benzene / 150 °C

With sodium azide; In d₇-N,N-dimethylformamide; 1,2-dichloro-benzene;

Reference yield:

: 6967-82-4
2-bromo-5-methylbenzoic acid

: 1420532-43-9
1-(2-bromo-5-methylbenzyl)-5-methyl-4-(trimethylsilyl)-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 4 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere; Reflux

2: phosphorus tribromide / diethyl ether / 3 h / 0 °C / Inert atmosphere

3: sodium azide / d₇-N,N-dimethylformamide / 80 °C

4: 1,2-dichloro-benzene / 150 °C

With lithium aluminium tetrahydride; sodium azide; phosphorus tribromide; In tetrahydrofuran; diethyl ether; d₇-N,N-dimethylformamide; 1,2-dichloro-benzene;