[(4R,5R)-5-(Hydroxy-diphenyl-methyl)-2-(4-hydroxymethyl-phenyl)-[1,3]dioxolan-4-yl]-diphenyl-methanol

Base Information

Chemical Name:[(4R,5R)-5-(Hydroxy-diphenyl-methyl)-2-(4-hydroxymethyl-phenyl)-[1,3]dioxolan-4-yl]-diphenyl-methanol
CAS No.:183057-89-8
Molecular Formula:C₃₆H₃₂O₅
Molecular Weight:544.647
Hs Code.:

Synonyms:[(4R,5R)-5-(Hydroxy-diphenyl-methyl)-2-(4-hydroxymethyl-phenyl)-[1,3]dioxolan-4-yl]-diphenyl-methanol

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Chemical Property of [(4R,5R)-5-(Hydroxy-diphenyl-methyl)-2-(4-hydroxymethyl-phenyl)-[1,3]dioxolan-4-yl]-diphenyl-methanol

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Technology Process of [(4R,5R)-5-(Hydroxy-diphenyl-methyl)-2-(4-hydroxymethyl-phenyl)-[1,3]dioxolan-4-yl]-diphenyl-methanol

There total 5 articles about [(4R,5R)-5-(Hydroxy-diphenyl-methyl)-2-(4-hydroxymethyl-phenyl)-[1,3]dioxolan-4-yl]-diphenyl-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 183057-64-9
4-(hydroxymethyl)benzaldehyde dimethyl acetal

: 183057-89-8
[(4R,5R)-5-(Hydroxy-diphenyl-methyl)-2-(4-hydroxymethyl-phenyl)-[1,3]dioxolan-4-yl]-diphenyl-methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / Et₃N / CH₂Cl₂ / 5 h / Ambient temperature

2: 74 percent / BF₃*OEt₂ / ethyl acetate / 7 h / Ambient temperature

3: 1.) Mg / 1.) THF; 2.) THF, r.t., 4 h

With boron trifluoride diethyl etherate; magnesium; triethylamine; In dichloromethane; ethyl acetate;
DOI:10.1002/hlca.19960790621

Reference yield:

: 42228-16-0
methyl 4-(dimethoxymethyl)benzoate

: 183057-89-8
[(4R,5R)-5-(Hydroxy-diphenyl-methyl)-2-(4-hydroxymethyl-phenyl)-[1,3]dioxolan-4-yl]-diphenyl-methanol

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / LiAlH₄ / diethyl ether / 1 h / Ambient temperature

2: 99 percent / Et₃N / CH₂Cl₂ / 5 h / Ambient temperature

3: 74 percent / BF₃*OEt₂ / ethyl acetate / 7 h / Ambient temperature

4: 1.) Mg / 1.) THF; 2.) THF, r.t., 4 h

With lithium aluminium tetrahydride; boron trifluoride diethyl etherate; magnesium; triethylamine; In diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1002/hlca.19960790621

Reference yield:

: 183057-67-2
Benzoic acid 4-dimethoxymethyl-benzyl ester

: 183057-89-8
[(4R,5R)-5-(Hydroxy-diphenyl-methyl)-2-(4-hydroxymethyl-phenyl)-[1,3]dioxolan-4-yl]-diphenyl-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / BF₃*OEt₂ / ethyl acetate / 7 h / Ambient temperature

2: 1.) Mg / 1.) THF; 2.) THF, r.t., 4 h

With boron trifluoride diethyl etherate; magnesium; In ethyl acetate;
DOI:10.1002/hlca.19960790621