2-(methylsulfonyloxy)-3-[(tert-butyldiphenylsilyl)oxy]-4-methoxybenzaldehyde

Base Information

Chemical Name:2-(methylsulfonyloxy)-3-[(tert-butyldiphenylsilyl)oxy]-4-methoxybenzaldehyde
CAS No.:1242074-20-9
Molecular Formula:C₂₅H₂₈O₆SSi
Molecular Weight:484.645
Hs Code.:

Synonyms:2-(methylsulfonyloxy)-3-[(tert-butyldiphenylsilyl)oxy]-4-methoxybenzaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(methylsulfonyloxy)-3-[(tert-butyldiphenylsilyl)oxy]-4-methoxybenzaldehyde

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Technology Process of 2-(methylsulfonyloxy)-3-[(tert-butyldiphenylsilyl)oxy]-4-methoxybenzaldehyde

There total 1 articles about 2-(methylsulfonyloxy)-3-[(tert-butyldiphenylsilyl)oxy]-4-methoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1242060-69-0
2-hydroxy-3-[(tert-butyldiphenylsilyl)oxy]-4-methoxybenzaldehyde

: 124-63-0
methanesulfonyl chloride

: 1242074-20-9
2-(methylsulfonyloxy)-3-[(tert-butyldiphenylsilyl)oxy]-4-methoxybenzaldehyde

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 ℃; Inert atmosphere;
DOI:10.1021/np100108e

Reference yield: 78.0%

: 1242074-20-9
2-(methylsulfonyloxy)-3-[(tert-butyldiphenylsilyl)oxy]-4-methoxybenzaldehyde

: 61240-20-8
triphenyl-(3,4,5-trimethoxybenzyl)phosphonium bromide

: 1231184-87-4
C₃₅H₄₀O₈SSi

Guidance literature:: triphenyl-(3,4,5-trimethoxybenzyl)phosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 - 20 ℃; Inert atmosphere;

2-(methylsulfonyloxy)-3-[(tert-butyldiphenylsilyl)oxy]-4-methoxybenzaldehyde; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/np100108e