(4β,5α)-12-Hydroxy-N-[(1-phenylcyclohexyl)methyl]podocarpa-8,11,13-trien-16-amide

Base Information

• Chemical Name: (4β,5α)-12-Hydroxy-N-[(1-phenylcyclohexyl)methyl]podocarpa-8,11,13-trien-16-amide
• CAS No.: 551944-07-1
• Molecular Formula: C₃₀H₃₉NO₂
• Molecular Weight: 445.645

Synonyms:(4β,5α)-12-Hydroxy-N-[(1-phenylcyclohexyl)methyl]podocarpa-8,11,13-trien-16-amide

Chemical Property of (4β,5α)-12-Hydroxy-N-[(1-phenylcyclohexyl)methyl]podocarpa-8,11,13-trien-16-amide

Chemical Property:

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Technology Process of (4β,5α)-12-Hydroxy-N-[(1-phenylcyclohexyl)methyl]podocarpa-8,11,13-trien-16-amide

There total 2 articles about (4β,5α)-12-Hydroxy-N-[(1-phenylcyclohexyl)methyl]podocarpa-8,11,13-trien-16-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

podocarpic acid (5947-49-9) + 1-amino-2-phenyl-2,2-pentamethyleneethane (17380-54-0) + (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate (56602-33-6) → (4β,5α)-12-Hydroxy-N-[(1-phenylcyclohexyl)methyl]podocarpa-8,11,13-trien-16-amide (551944-07-1)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In water; N,N-dimethyl-formamide;

Reference yield:

podocarpic acid (5947-49-9) + 1-amino-2-phenyl-2,2-pentamethyleneethane (17380-54-0) → (4β,5α)-12-Hydroxy-N-[(1-phenylcyclohexyl)methyl]podocarpa-8,11,13-trien-16-amide (551944-07-1)

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;

DOI:10.1016/j.bmcl.2005.06.100

Reference yield:

(4β,5α)-12-Hydroxy-N-[(1-phenylcyclohexyl)methyl]podocarpa-8,11,13-trien-16-amide (551944-07-1) + diethyl chlorophosphate (814-49-3) → diethyl (4β,5α)-16-oxo-16-{[(1-phenylcyclohexyl)methyl]amino}podocarpa-8,11,13-trien-12-yl phosphate (551944-37-7)

Guidance literature:

With sodium hydride; In tetrahydrofuran;

DOI:10.1016/j.bmcl.2005.06.100

upstream raw materials:

podocarpic acid

1-amino-2-phenyl-2,2-pentamethyleneethane

(benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate

Downstream raw materials:

diethyl (4β,5α)-16-oxo-16-{[(1-phenylcyclohexyl)methyl]amino}podocarpa-8,11,13-trien-12-yl phosphate

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