C₁₉H₂₆O₅S

Base Information

Chemical Name:C₁₉H₂₆O₅S
CAS No.:948297-42-5
Molecular Formula:C₁₉H₂₆O₅S
Molecular Weight:366.478
Hs Code.:

C<sub>19</sub>H<sub>26</sub>O<sub>5</sub>S

Synonyms:C₁₉H₂₆O₅S

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Chemical Property of C₁₉H₂₆O₅S

Chemical Property:

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Technology Process of C₁₉H₂₆O₅S

There total 9 articles about C₁₉H₂₆O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₂₈O₄S

: 948297-42-5
C₁₉H₂₆O₅S

Guidance literature:: Multi-step reaction with 9 steps

1.1: 4-dimethylaminopyridine; pyridine / CH₂Cl₂

2.1: (S)-1-Me-3,3-diPh-tetrahydropyrrolo[1,2-c][1,3,2]oxazaborole; BH₃*SMe₂ / tetrahydrofuran / 0 °C

3.1: H₂; pyridine / Pd/CaCO₃/Pb / benzene / 760.05 Torr

3.2: 4-dimethylaminopyridine; imidazole / dimethylformamide

4.1: K₂CO₃ / methanol

5.1: SO₃*pyridine; dimethylsulfoxide; iPr₂NEt / CH₂Cl₂ / -25 °C

6.1: 74 percent / HF*pyridine; pyridine / tetrahydrofuran / 0 °C

7.1: 92 percent / pyridinium p-toluenesulfonate; HC(OMe)3 / CH₂Cl₂ / -10 °C

8.1: 88 percent / H₂O₂; [(NH₄)6Mo₇O₂₄] / methanol / 0 °C

9.1: 92 percent / LiAlH₄ / diethyl ether / -20 °C

With pyridine; dmap; lithium aluminium tetrahydride; pyridine-SO₃ complex; dimethylsulfide borane complex; hydrogen; dihydrogen peroxide; pyridinium p-toluenesulfonate; potassium carbonate; pyridine hydrogenfluoride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; trimethyl orthoformate; Lindlar's catalyst; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; benzene; 2.1: Corey-Bakshi-Shibata reduction / 5.1: Parikh-Doering oxidation;
DOI:10.1002/anie.200701515

Reference yield:

: 948297-18-5
C₁₂H₂₁NO₄

: 948297-42-5
C₁₉H₂₆O₅S

Guidance literature:: Multi-step reaction with 10 steps

1.1: n-BuLi / diethyl ether / -78 °C

1.2: MgBr₂*OEt₂ / diethyl ether / -78 - 0 °C

1.3: THF / diethyl ether / 20 °C

2.1: 4-dimethylaminopyridine; pyridine / CH₂Cl₂

3.1: (S)-1-Me-3,3-diPh-tetrahydropyrrolo[1,2-c][1,3,2]oxazaborole; BH₃*SMe₂ / tetrahydrofuran / 0 °C

4.1: H₂; pyridine / Pd/CaCO₃/Pb / benzene / 760.05 Torr

4.2: 4-dimethylaminopyridine; imidazole / dimethylformamide

5.1: K₂CO₃ / methanol

6.1: SO₃*pyridine; dimethylsulfoxide; iPr₂NEt / CH₂Cl₂ / -25 °C

7.1: 74 percent / HF*pyridine; pyridine / tetrahydrofuran / 0 °C

8.1: 92 percent / pyridinium p-toluenesulfonate; HC(OMe)3 / CH₂Cl₂ / -10 °C

9.1: 88 percent / H₂O₂; [(NH₄)6Mo₇O₂₄] / methanol / 0 °C

10.1: 92 percent / LiAlH₄ / diethyl ether / -20 °C

With pyridine; dmap; lithium aluminium tetrahydride; n-butyllithium; pyridine-SO₃ complex; dimethylsulfide borane complex; hydrogen; dihydrogen peroxide; pyridinium p-toluenesulfonate; potassium carbonate; pyridine hydrogenfluoride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; trimethyl orthoformate; Lindlar's catalyst; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; benzene; 3.1: Corey-Bakshi-Shibata reduction / 6.1: Parikh-Doering oxidation;
DOI:10.1002/anie.200701515

Reference yield:

: 27098-65-3
3-phenylsulfanyl-propionaldehyde

: 948297-42-5
C₁₉H₂₆O₅S

Guidance literature:: Multi-step reaction with 11 steps

1.1: diethyl ether / 0 °C

2.1: n-BuLi / diethyl ether / -78 °C

2.2: MgBr₂*OEt₂ / diethyl ether / -78 - 0 °C

2.3: THF / diethyl ether / 20 °C

3.1: 4-dimethylaminopyridine; pyridine / CH₂Cl₂

4.1: (S)-1-Me-3,3-diPh-tetrahydropyrrolo[1,2-c][1,3,2]oxazaborole; BH₃*SMe₂ / tetrahydrofuran / 0 °C

5.1: H₂; pyridine / Pd/CaCO₃/Pb / benzene / 760.05 Torr

5.2: 4-dimethylaminopyridine; imidazole / dimethylformamide

6.1: K₂CO₃ / methanol

7.1: SO₃*pyridine; dimethylsulfoxide; iPr₂NEt / CH₂Cl₂ / -25 °C

8.1: 74 percent / HF*pyridine; pyridine / tetrahydrofuran / 0 °C

9.1: 92 percent / pyridinium p-toluenesulfonate; HC(OMe)3 / CH₂Cl₂ / -10 °C

10.1: 88 percent / H₂O₂; [(NH₄)6Mo₇O₂₄] / methanol / 0 °C

11.1: 92 percent / LiAlH₄ / diethyl ether / -20 °C

With pyridine; dmap; lithium aluminium tetrahydride; n-butyllithium; pyridine-SO₃ complex; dimethylsulfide borane complex; hydrogen; dihydrogen peroxide; pyridinium p-toluenesulfonate; potassium carbonate; pyridine hydrogenfluoride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; trimethyl orthoformate; Lindlar's catalyst; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; benzene; 4.1: Corey-Bakshi-Shibata reduction / 7.1: Parikh-Doering oxidation;
DOI:10.1002/anie.200701515