(1S,2R,3S,4R)-7-cyclohexylidene-2,3-di(hydroxymethyl)bicyclo[2.2.1]hept-5-ene acetonide

Base Information

Chemical Name:(1S*,2R*,3S*,4R*)-7-cyclohexylidene-2,3-di(hydroxymethyl)bicyclo[2.2.1]hept-5-ene acetonide
CAS No.:1190404-24-0
Molecular Formula:C₁₈H₂₆O₂
Molecular Weight:274.403
Hs Code.:

Synonyms:(1S*,2R*,3S*,4R*)-7-cyclohexylidene-2,3-di(hydroxymethyl)bicyclo[2.2.1]hept-5-ene acetonide

Suppliers and Price of (1S*,2R*,3S*,4R*)-7-cyclohexylidene-2,3-di(hydroxymethyl)bicyclo[2.2.1]hept-5-ene acetonide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S*,2R*,3S*,4R*)-7-cyclohexylidene-2,3-di(hydroxymethyl)bicyclo[2.2.1]hept-5-ene acetonide

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Technology Process of (1S*,2R*,3S*,4R*)-7-cyclohexylidene-2,3-di(hydroxymethyl)bicyclo[2.2.1]hept-5-ene acetonide

There total 1 articles about (1S*,2R*,3S*,4R*)-7-cyclohexylidene-2,3-di(hydroxymethyl)bicyclo[2.2.1]hept-5-ene acetonide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 116-11-0
2-Methoxypropene

: 1190404-23-9
(1S*,2R*,3S*,4R*)-7-cyclohexylidene-2,3-di(hydroxymethyl)bicyclo[2.2.1]hept-5-ene

: 1190404-24-0
(1S*,2R*,3S*,4R*)-7-cyclohexylidene-2,3-di(hydroxymethyl)bicyclo[2.2.1]hept-5-ene acetonide

Guidance literature:: With camphor-10-sulfonic acid; In dichloromethane; for 6h; Inert atmosphere;
DOI:10.1016/j.tet.2009.07.016

Reference yield: 56.0%

: 1190404-24-0
(1S*,2R*,3S*,4R*)-7-cyclohexylidene-2,3-di(hydroxymethyl)bicyclo[2.2.1]hept-5-ene acetonide

: 1190404-25-1
(cis,cis,cis)-1-cyclohexylidene-2,3,4,5-tetra-(hydroxymethyl)cyclopentane acetonide

Guidance literature:: (1S*,2R*,3S*,4R*)-7-cyclohexylidene-2,3-di(hydroxymethyl)bicyclo[2.2.1]hept-5-ene acetonide; With pyridine; ozone; In dichloromethane; at -60 ℃;

With sodium tetrahydroborate; In ethanol; dichloromethane; at -80 - 20 ℃;

With water; In ethanol; dichloromethane;
DOI:10.1016/j.tet.2009.07.016