M-1-(2'-benzyloxy-4',6'-dimethylphenyl)-2-(N-methylaminomethyl)naphthalene

Base Information

Chemical Name:M-1-(2'-benzyloxy-4',6'-dimethylphenyl)-2-(N-methylaminomethyl)naphthalene
CAS No.:210490-10-1
Molecular Formula:C₂₇H₂₇NO
Molecular Weight:381.517
Hs Code.:

Synonyms:M-1-(2'-benzyloxy-4',6'-dimethylphenyl)-2-(N-methylaminomethyl)naphthalene

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Chemical Property of M-1-(2'-benzyloxy-4',6'-dimethylphenyl)-2-(N-methylaminomethyl)naphthalene

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Technology Process of M-1-(2'-benzyloxy-4',6'-dimethylphenyl)-2-(N-methylaminomethyl)naphthalene

There total 6 articles about M-1-(2'-benzyloxy-4',6'-dimethylphenyl)-2-(N-methylaminomethyl)naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 593-51-1
methylamine hydrochloride

: 210489-23-9,210490-09-8,210490-20-3
M-1-(2'-benzyloxy-4',6'-dimethylphenyl)-2-bromomethylnaphthalene

: 210490-10-1
M-1-(2'-benzyloxy-4',6'-dimethylphenyl)-2-(N-methylaminomethyl)naphthalene

Guidance literature:: With methylamine; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1016/S0957-4166(98)00020-2

Reference yield:

: 138435-72-0
(±)-1,3-dimethyl-6H-benzo[b]naphtho[1,2-d]pyranone

: 210490-10-1
M-1-(2'-benzyloxy-4',6'-dimethylphenyl)-2-(N-methylaminomethyl)naphthalene

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaH / 1.) Et₂O, RT, 30 min, 2.) Et₂O, RT

2: Cs₂CO₃ / acetone / 12 h / Ambient temperature

3: LiAlH₄ / tetrahydrofuran / 1 h / Ambient temperature

4: (CCl₂Br)2, Ph₃P / CH₂Cl₂ / 0.5 h / Ambient temperature

5: 99 percent / MeNH₂ / CH₂Cl₂ / 1 h / Ambient temperature

With lithium aluminium tetrahydride; 1,2-dibromo-1,1,2,2-tetrachloroethane; sodium hydride; caesium carbonate; triphenylphosphine; methylamine; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1016/S0957-4166(98)00020-2

Reference yield:

: 1-(2-Hydroxy-4,6-dimethyl-phenyl)-naphthalene-2-carboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

: 210490-10-1
M-1-(2'-benzyloxy-4',6'-dimethylphenyl)-2-(N-methylaminomethyl)naphthalene

Guidance literature:: Multi-step reaction with 4 steps

1: Cs₂CO₃ / acetone / 12 h / Ambient temperature

2: LiAlH₄ / tetrahydrofuran / 1 h / Ambient temperature

3: (CCl₂Br)2, Ph₃P / CH₂Cl₂ / 0.5 h / Ambient temperature

4: 99 percent / MeNH₂ / CH₂Cl₂ / 1 h / Ambient temperature

With lithium aluminium tetrahydride; 1,2-dibromo-1,1,2,2-tetrachloroethane; caesium carbonate; triphenylphosphine; methylamine; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1016/S0957-4166(98)00020-2