[meso-5α,10α,15α-tris(o-pivalamidophenyl)-20β-(o-((3-(N-imidazolyl)propyl)ureido)phenyl)porphyrinato]iron(II)

Base Information

Chemical Name:[meso-5α,10α,15α-tris(o-pivalamidophenyl)-20β-(o-((3-(N-imidazolyl)propyl)ureido)phenyl)porphyrinato]iron(II)
CAS No.:84849-06-9
Molecular Formula:C₆₆H₆₅FeN₁₁O₄
Molecular Weight:1132.16
Hs Code.:

Synonyms:[meso-5α,10α,15α-tris(o-pivalamidophenyl)-20β-(o-((3-(N-imidazolyl)propyl)ureido)phenyl)porphyrinato]iron(II)

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Chemical Property of [meso-5α,10α,15α-tris(o-pivalamidophenyl)-20β-(o-((3-(N-imidazolyl)propyl)ureido)phenyl)porphyrinato]iron(II)

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Technology Process of [meso-5α,10α,15α-tris(o-pivalamidophenyl)-20β-(o-((3-(N-imidazolyl)propyl)ureido)phenyl)porphyrinato]iron(II)

There total 1 articles about [meso-5α,10α,15α-tris(o-pivalamidophenyl)-20β-(o-((3-(N-imidazolyl)propyl)ureido)phenyl)porphyrinato]iron(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 75526-89-5
meso-5α,10α,15α-tris(o-pivalamidophenyl)-20β-(o-((3-(N-imidazolyl)propyl)ureido)phenyl)porphyrin

: 7789-46-0
iron(II) bromide

: 84849-06-9
[meso-5α,10α,15α-tris(o-pivalamidophenyl)-20β-(o-((3-(N-imidazolyl)propyl)ureido)phenyl)porphyrinato]iron(II)

Guidance literature:: With 2,6-dimethylpyridine; In tetrahydrofuran; benzene; byproducts: 2,6-lutidine hydrobromide; 1 equiv of ligand was dissolved in benzene, THF and 10 equiv of 2,6-lutidine, 5 equiv of anhyd. FeBr2 was added, heated at reflux for 25 min; solvent removed in vac., chromd. on neutral Al2O3 (MeOH-toluene), brought to dryness in vac., dissolved in min. of THF, pptd. by adding heptane;

Reference yield:

: 84849-06-9
[meso-5α,10α,15α-tris(o-pivalamidophenyl)-20β-(o-((3-(N-imidazolyl)propyl)ureido)phenyl)porphyrinato]iron(II)

: [meso-5α,10α,15α-tris(o-pivalamidophenyl)-20β-(o-((3-(N-imidazolyl)propyl)ureido)phenyl)porphyrinato]iron(II)(O2)

Guidance literature:: With oxygen; In toluene; under N2, deoxygenated soln. of Fe-compd. in toluene was treated with O2 at 25°C; followed spectrophotometrically; Kinetics;

Reference yield:

: 84849-06-9
[meso-5α,10α,15α-tris(o-pivalamidophenyl)-20β-(o-((3-(N-imidazolyl)propyl)ureido)phenyl)porphyrinato]iron(II)

: [meso-5α,10α,15α-tris(o-pivalamidophenyl)-20β-(o-((3-(N-imidazolyl)propyl)ureido)phenyl)porphyrinato]iron(II)(CO)

Guidance literature:: With carbon monoxide; In toluene; under N2, deoxygenated soln. of Fe-compd. in toluene was treated with CO at 25°C; followed spectrophotometrically; Kinetics;