meso-5α,10α,15α-tris(o-pivalamidophenyl)-20β-(o-((3-(N-imidazolyl)propyl)ureido)phenyl)porphyrin

Base Information

• Chemical Name: meso-5α,10α,15α-tris(o-pivalamidophenyl)-20β-(o-((3-(N-imidazolyl)propyl)ureido)phenyl)porphyrin
• CAS No.: 75526-89-5
• Molecular Formula: C₆₆H₆₇N₁₁O₄
• Molecular Weight: 1078.33

Synonyms:meso-5α,10α,15α-tris(o-pivalamidophenyl)-20β-(o-((3-(N-imidazolyl)propyl)ureido)phenyl)porphyrin

Chemical Property of meso-5α,10α,15α-tris(o-pivalamidophenyl)-20β-(o-((3-(N-imidazolyl)propyl)ureido)phenyl)porphyrin

Chemical Property:

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Technology Process of meso-5α,10α,15α-tris(o-pivalamidophenyl)-20β-(o-((3-(N-imidazolyl)propyl)ureido)phenyl)porphyrin

There total 3 articles about meso-5α,10α,15α-tris(o-pivalamidophenyl)-20β-(o-((3-(N-imidazolyl)propyl)ureido)phenyl)porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrakis-5,10,15,20-(o-aminophenyl)porphyrin (52199-35-6) → meso-tri(α,α,α-o-pivalamidophenyl)-β-o-3-(N-imidazolyl)propylureidophenylporphyrin (75526-89-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) pyridine, 2.) 10percent NH₄OH / 1.) CH₂Cl₂, 8 h, 2.) 2 h

2: 2.) pyridine / 1.) THF, 20 min, 2.) 2 h

With pyridine; ammonium hydroxide;

DOI:10.1021/ja00532a033

Reference yield:

pivaloyl chloride (3282-30-2) → meso-tri(α,α,α-o-pivalamidophenyl)-β-o-3-(N-imidazolyl)propylureidophenylporphyrin (75526-89-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) pyridine, 2.) 10percent NH₄OH / 1.) CH₂Cl₂, 8 h, 2.) 2 h

2: 2.) pyridine / 1.) THF, 20 min, 2.) 2 h

With pyridine; ammonium hydroxide;

DOI:10.1021/ja00532a033

Reference yield:

phosgene (75-44-5) + 3-(1H-imidazol-1-yl)propan-1-amine (5036-48-6) + meso-α-mono(o-aminophenyl)-α,α,α-tri(o-pivalamidophenyl)porphyrin (75557-89-0) → meso-tri(α,α,α-o-pivalamidophenyl)-β-o-3-(N-imidazolyl)propylureidophenylporphyrin (75526-89-5)

Guidance literature:

With pyridine; Yield given. Multistep reaction; 1.) THF, 20 min, 2.) 2 h;

DOI:10.1021/ja00532a033

upstream raw materials:

phosgene

3-(1H-imidazol-1-yl)propan-1-amine

meso-α-mono(o-aminophenyl)-α,α,α-tri(o-pivalamidophenyl)porphyrin

tetrakis-5,10,15,20-(o-aminophenyl)porphyrin

Downstream raw materials:

[meso-5α,10α,15α-tris(o-pivalamidophenyl)-20β-(o-((3-(N-imidazolyl)propyl)ureido)phenyl)porphyrinato]iron(II)

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