3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-amine

Base Information

Chemical Name:3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-amine
CAS No.:1024005-13-7
Molecular Formula:C₁₄H₁₃F₂N₃
Molecular Weight:261.274
Hs Code.:

3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2<sup>(6)</sup>,4-dien-5-amine

Synonyms:3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-amine

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Chemical Property of 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-amine

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Technology Process of 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-amine

There total 1 articles about 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 916591-87-2,916591-89-4,916591-88-3
3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-carboxylic acid

: 1024005-13-7
3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-amine

Guidance literature:: 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-carboxylic acid; With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; In 1,4-dioxane; at 20 - 35 ℃; for 0.333333h;

With sodium azide; tetrabutylammomium bromide; In 1,4-dioxane; for 1h;

With sulfuric acid; water; In 1,4-dioxane; at 100 ℃; for 2h;

Reference yield: 49.0%

: 1024005-13-7
3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-amine

: 100-39-0
benzyl bromide

: 1024003-70-0
N₅,N₅-dibenzyl-3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-amine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 - 35 ℃; for 8 - 16h;

Reference yield: 45.0%

: 1024005-13-7
3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-amine

: 1024005-17-1
5-iodo-3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene

Guidance literature:: 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-amine; With hydrogenchloride; sodium nitrite; In diethyl ether; water; at 0 - 10 ℃; for 0.25h;

With potassium iodide; In diethyl ether; water; at 20 - 90 ℃; for 3h;