methoxycarbonylmethyl 6-O-acetyl-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

Base Information

Chemical Name:methoxycarbonylmethyl 6-O-acetyl-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside
CAS No.:441017-60-3
Molecular Formula:C₃₂H₃₆O₈S
Molecular Weight:580.699
Hs Code.:

Synonyms:methoxycarbonylmethyl 6-O-acetyl-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

Suppliers and Price of methoxycarbonylmethyl 6-O-acetyl-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of methoxycarbonylmethyl 6-O-acetyl-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methoxycarbonylmethyl 6-O-acetyl-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

There total 3 articles about methoxycarbonylmethyl 6-O-acetyl-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 4356-77-8
acetyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 2365-48-2
Methyl thioglycolate

: 441017-60-3
methoxycarbonylmethyl 6-O-acetyl-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

: methoxycarbonylmethyl 6-O-acetyl-2,3,4-tri-O-benzyl-1-thio-β-D-glucopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 20 ℃; for 4h;

Reference yield: 74.0%

: 4356-77-8
acetyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 2365-48-2
Methyl thioglycolate

: 441017-60-3
methoxycarbonylmethyl 6-O-acetyl-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1021/ol025887d

Reference yield:

: 3879-79-6,17791-37-6,19488-61-0,53008-63-2,61330-62-9,69237-94-1,69237-95-2,71526-33-5,83462-67-3,84799-77-9,103421-29-0,103421-30-3,139241-42-2
methyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

: 441017-60-3
methoxycarbonylmethyl 6-O-acetyl-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: ZnCl₂ / acetic acid / 4 h / 20 °C

2: 76 percent / BF₃*Et₂O / CH₂Cl₂ / 4 h / 0 - 20 °C

With boron trifluoride diethyl etherate; zinc(II) chloride; In dichloromethane; acetic acid;