BenzenesulfonaMide, N-(3,5-dibroMo-2-pyridinyl)-

Base Information Edit

Chemical Name:BenzenesulfonaMide, N-(3,5-dibroMo-2-pyridinyl)-
CAS No.:1111637-62-7
Molecular Formula:C₁₁H₈Br₂N₂O₂S
Molecular Weight:392.071
Hs Code.:
Mol file:1111637-62-7.mol

Synonyms:N-(3,5-dibromopyridin-2-yl)benzenesulfonamide

Suppliers and Price of BenzenesulfonaMide, N-(3,5-dibroMo-2-pyridinyl)-

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of BenzenesulfonaMide, N-(3,5-dibroMo-2-pyridinyl)- Edit

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of BenzenesulfonaMide, N-(3,5-dibroMo-2-pyridinyl)-

There total 1 articles about BenzenesulfonaMide, N-(3,5-dibroMo-2-pyridinyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 35486-42-1
2-amino-3,5-dibromopyridine

: 98-09-9
benzenesulfonyl chloride

: 1111637-62-7
N-(3,5-dibromopyridin-2-yl)benzenesulfonamide

Guidance literature:: 2-amino-3,5-dibromopyridine; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 25 ℃; for 1h; Inert atmosphere;

benzenesulfonyl chloride; In tetrahydrofuran; mineral oil; at 25 ℃; for 24h; Inert atmosphere;
DOI:10.1002/chem.201602519

Reference yield: 95.0%

: 1111637-62-7
N-(3,5-dibromopyridin-2-yl)benzenesulfonamide

: 133816-00-9
phenyl(trimethylsilylethynyl)iodonium triflate

: N-(3,5-dibromopyridin-2-yl)-N-[(trimethylsilyl)ethynyl]benzenesulfonamide

Guidance literature:: N-(3,5-dibromopyridin-2-yl)benzenesulfonamide; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at 0 ℃; for 1h; Inert atmosphere;

phenyl(trimethylsilylethynyl)iodonium triflate; In tetrahydrofuran; toluene; at 0 - 25 ℃; for 16h; Inert atmosphere;
DOI:10.1002/chem.201602519