(+/-)-4-nitro-3-phenylbutyric acid 4'-(4-nitro-3-phenylbutyryloxymethyl)-[2,2']bipyridinyl-4-ylmethyl ester

Base Information

Chemical Name:(+/-)-4-nitro-3-phenylbutyric acid 4'-(4-nitro-3-phenylbutyryloxymethyl)-[2,2']bipyridinyl-4-ylmethyl ester
CAS No.:866789-27-7
Molecular Formula:C₃₂H₃₀N₄O₈
Molecular Weight:598.612
Hs Code.:

Synonyms:(+/-)-4-nitro-3-phenylbutyric acid 4'-(4-nitro-3-phenylbutyryloxymethyl)-[2,2']bipyridinyl-4-ylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-4-nitro-3-phenylbutyric acid 4'-(4-nitro-3-phenylbutyryloxymethyl)-[2,2']bipyridinyl-4-ylmethyl ester

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of (+/-)-4-nitro-3-phenylbutyric acid 4'-(4-nitro-3-phenylbutyryloxymethyl)-[2,2']bipyridinyl-4-ylmethyl ester

There total 2 articles about (+/-)-4-nitro-3-phenylbutyric acid 4'-(4-nitro-3-phenylbutyryloxymethyl)-[2,2']bipyridinyl-4-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 866788-63-8
(diethoxyphosphoryl)acetic acid 4'-[(diethoxyphosphoryl)acetoxymethyl]-[2,2']bipyridinyl-4-ylmethyl ester

: 866789-27-7
(+/-)-4-nitro-3-phenylbutyric acid 4'-(4-nitro-3-phenylbutyryloxymethyl)-[2,2']bipyridinyl-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: t-BuOK / tetrahydrofuran / 0.25 h / 0 °C

1.2: 98 percent / tetrahydrofuran / 0 - 25 °C

2.1: 78 percent / TBAF / tetrahydrofuran / -10 - 20 °C

With potassium tert-butylate; tetrabutyl ammonium fluoride; In tetrahydrofuran; 1.2: Horner-Emmons reaction;
DOI:10.1039/b503778f

Reference yield:

: 109073-77-0
4,4'-bis(hydroxymethyl)-2,2'-bipyridine

: 866789-27-7
(+/-)-4-nitro-3-phenylbutyric acid 4'-(4-nitro-3-phenylbutyryloxymethyl)-[2,2']bipyridinyl-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 85 percent / diisopropylcarbodiimide / CH₂Cl₂; tetrahydrofuran / 0.33 h / 100 °C / microwave irradiation

2.1: t-BuOK / tetrahydrofuran / 0.25 h / 0 °C

2.2: 98 percent / tetrahydrofuran / 0 - 25 °C

3.1: 78 percent / TBAF / tetrahydrofuran / -10 - 20 °C

With potassium tert-butylate; tetrabutyl ammonium fluoride; diisopropyl-carbodiimide; In tetrahydrofuran; dichloromethane; 2.2: Horner-Emmons reaction;
DOI:10.1039/b503778f