4,9-bis(p-tolylsulphonyl)benz-15,18,23-trioxa-1,4,9,12-tetra-azabicyclo<10.8.5>pentacosane

Base Information

Chemical Name:4,9-bis(p-tolylsulphonyl)benz-15,18,23-trioxa-1,4,9,12-tetra-azabicyclo<10.8.5>pentacosane
CAS No.:121031-85-4
Molecular Formula:C₃₆H₅₀N₄O₇S₂
Molecular Weight:714.948
Hs Code.:

4,9-bis(p-tolylsulphonyl)benz<f>-15,18,23-trioxa-1,4,9,12-tetra-azabicyclo<10.8.5>pentacosane

Synonyms:4,9-bis(p-tolylsulphonyl)benz-15,18,23-trioxa-1,4,9,12-tetra-azabicyclo<10.8.5>pentacosane

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Chemical Property of 4,9-bis(p-tolylsulphonyl)benz-15,18,23-trioxa-1,4,9,12-tetra-azabicyclo<10.8.5>pentacosane

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Technology Process of 4,9-bis(p-tolylsulphonyl)benz-15,18,23-trioxa-1,4,9,12-tetra-azabicyclo<10.8.5>pentacosane

There total 4 articles about 4,9-bis(p-tolylsulphonyl)benz-15,18,23-trioxa-1,4,9,12-tetra-azabicyclo<10.8.5>pentacosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 113917-86-5
7,13-bis<2-(tolylsulphonylamino)ethyl>-1,4,10-trioxa-7,13-diazacyclopentadecane

: 91-13-4
α,α'-dibromo-o-xylene

: 121031-85-4
4,9-bis(p-tolylsulphonyl)benz-15,18,23-trioxa-1,4,9,12-tetra-azabicyclo<10.8.5>pentacosane

Guidance literature:: With sodium hydroxide; tetra-(n-butyl)ammonium iodide; Heating;

Reference yield:

: 31249-95-3
Kryptofix 21

: 121031-85-4
4,9-bis(p-tolylsulphonyl)benz-15,18,23-trioxa-1,4,9,12-tetra-azabicyclo<10.8.5>pentacosane

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / acetonitrile / Heating

2: 76 percent / 45percent aq. NaOH, tetrabutylammonium iodide / Heating

With sodium hydroxide; tetra-(n-butyl)ammonium iodide; In acetonitrile;

Reference yield:

: 31255-10-4
1,2-bis-(2-bromo-ethoxy)-ethane

: 121031-85-4
4,9-bis(p-tolylsulphonyl)benz-15,18,23-trioxa-1,4,9,12-tetra-azabicyclo<10.8.5>pentacosane

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / Bu₄NI, 50 percent aq. NaOH / toluene / 10 h / Heating

2: 88 percent / LiAlH₄ / tetrahydrofuran / 20 h / Heating

3: 96 percent / acetonitrile / 1 h / Heating

4: 76 percent / Bu₄NI, 50 percent aq. NaOH / toluene / 16 h / Heating

With sodium hydroxide; lithium aluminium tetrahydride; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; toluene; acetonitrile;