1R(1,2,4,6/3,5)-7-O-acetyl-1,2-anhydro-3,4,5-tri-O-benzyl-6-hydroxymethylcyclohexane-1,2,3,4,5-pentol

Base Information

Chemical Name:1R(1,2,4,6/3,5)-7-O-acetyl-1,2-anhydro-3,4,5-tri-O-benzyl-6-hydroxymethylcyclohexane-1,2,3,4,5-pentol
CAS No.:157761-59-6
Molecular Formula:C₃₀H₃₂O₆
Molecular Weight:488.58
Hs Code.:

Synonyms:1R(1,2,4,6/3,5)-7-O-acetyl-1,2-anhydro-3,4,5-tri-O-benzyl-6-hydroxymethylcyclohexane-1,2,3,4,5-pentol

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Chemical Property of 1R(1,2,4,6/3,5)-7-O-acetyl-1,2-anhydro-3,4,5-tri-O-benzyl-6-hydroxymethylcyclohexane-1,2,3,4,5-pentol

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Technology Process of 1R(1,2,4,6/3,5)-7-O-acetyl-1,2-anhydro-3,4,5-tri-O-benzyl-6-hydroxymethylcyclohexane-1,2,3,4,5-pentol

There total 3 articles about 1R(1,2,4,6/3,5)-7-O-acetyl-1,2-anhydro-3,4,5-tri-O-benzyl-6-hydroxymethylcyclohexane-1,2,3,4,5-pentol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 157761-57-4
(1R,2R,3S,4R,6R)-2,3,4-Tris-benzyloxy-5-methylene-7-oxa-bicyclo[4.1.0]heptane

: 157761-59-6
1R(1,2,4,6/3,5)-7-O-acetyl-1,2-anhydro-3,4,5-tri-O-benzyl-6-hydroxymethylcyclohexane-1,2,3,4,5-pentol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) B₂H₆, 2.) 2 N aq. NaOH, 30percent aq. H₂O₂ / 1.) THF, 2.) THF, RT, 30 min

2: pyridine

With pyridine; sodium hydroxide; dihydrogen peroxide; diborane;
DOI:10.1055/s-1997-1292

Reference yield:

: 102997-56-8
1R(1,2,4/3,5)-1,2-anhydro-3,4,5-tri-O-benzyl-6-enecyclohexane-1,2,3,4,5-pentol

: 157761-59-6
1R(1,2,4,6/3,5)-7-O-acetyl-1,2-anhydro-3,4,5-tri-O-benzyl-6-hydroxymethylcyclohexane-1,2,3,4,5-pentol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) BuLi / 1.) THF, hexane, 2.) THF, hexane, RT, 15 min

2: 1.) B₂H₆, 2.) 2 N aq. NaOH, 30percent aq. H₂O₂ / 1.) THF, 2.) THF, RT, 30 min

3: pyridine

With pyridine; sodium hydroxide; n-butyllithium; dihydrogen peroxide; diborane;
DOI:10.1055/s-1997-1292