C₄₂H₅₇N₅O₆

Base Information

Chemical Name:C₄₂H₅₇N₅O₆
CAS No.:680620-91-1
Molecular Formula:C₄₂H₅₇N₅O₆
Molecular Weight:727.944
Hs Code.:

C<sub>42</sub>H<sub>57</sub>N<sub>5</sub>O<sub>6</sub>

Synonyms:C₄₂H₅₇N₅O₆

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Chemical Property of C₄₂H₅₇N₅O₆

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Technology Process of C₄₂H₅₇N₅O₆

There total 15 articles about C₄₂H₅₇N₅O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.5%

: 680620-90-0
C₄₅H₆₅N₅O₆Si

: 680620-91-1
C₄₂H₅₇N₅O₆

Guidance literature:: With potassium carbonate; In methanol; dichloromethane; at 20 ℃; for 0.166667h;
DOI:10.1021/ja039416d

Reference yield:

: 99072-43-2
methyl 5-acetamido-2-nitrobenzoate

: 680620-91-1
C₄₂H₅₇N₅O₆

Guidance literature:: Multi-step reaction with 11 steps

1.1: 92.3 percent / H₂SO₄ / methanol / 0.5 h / Heating

2.1: 78.3 percent / ICl; AcOH / 12 h

3.1: 93.8 percent / H₂SO₄ / CH₂Cl₂ / 1 h / 20 °C

4.1: 84.8 percent / AcOH / Fe / ethanol / 2 h / Heating

5.1: aq. NaNO₂; aq. HCl / acetonitrile / 0.5 h / 0 °C

5.2: 86.2 percent / K₂CO₃ / acetonitrile; H₂O / 0 - 20 °C

6.1: 93.8 percent / aq. NaOH / methanol / 0.5 h / Heating

7.1: 85.3 percent / DCC; DMAP / CH₂Cl₂ / 48 h / 20 °C

8.1: 93.8 percent / Pd(PPh₃)2Cl₂; CuI; Et₃N / 12 h / 40 °C

9.1: 90.2 percent / K₂CO₃ / methanol / 0.08 h / 20 °C

10.1: 88.9 percent / Pd(dba)2; CuI; PPh₃ / Et₃N / 24 h / 70 °C

11.1: 96.5 percent / K₂CO₃ / methanol; CH₂Cl₂ / 0.17 h / 20 °C

With hydrogenchloride; dmap; bis-triphenylphosphine-palladium(II) chloride; sodium hydroxide; copper(l) iodide; sulfuric acid; Iodine monochloride; potassium carbonate; acetic acid; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; sodium nitrite; iron; triethylamine; In methanol; ethanol; dichloromethane; acetonitrile; 8.1: Sonogashira coupling / 10.1: Sonogashira coupling;
DOI:10.1021/ja039416d

Reference yield:

: 111-87-5
octanol

: 680620-91-1
C₄₂H₅₇N₅O₆

Guidance literature:: Multi-step reaction with 5 steps

1: 85.3 percent / DCC; DMAP / CH₂Cl₂ / 48 h / 20 °C

2: 93.8 percent / Pd(PPh₃)2Cl₂; CuI; Et₃N / 12 h / 40 °C

3: 90.2 percent / K₂CO₃ / methanol / 0.08 h / 20 °C

4: 88.9 percent / Pd(dba)2; CuI; PPh₃ / Et₃N / 24 h / 70 °C

5: 96.5 percent / K₂CO₃ / methanol; CH₂Cl₂ / 0.17 h / 20 °C

With dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; triethylamine; In methanol; dichloromethane; 2: Sonogashira coupling / 4: Sonogashira coupling;
DOI:10.1021/ja039416d