N-[(4-methylphenyl)-sulfonyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl diphenylphosphinate

Base Information

Chemical Name:N-[(4-methylphenyl)-sulfonyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl diphenylphosphinate
CAS No.:960059-42-1
Molecular Formula:C₂₅H₂₆NO₄PS
Molecular Weight:467.525
Hs Code.:

Synonyms:N-[(4-methylphenyl)-sulfonyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl diphenylphosphinate

Suppliers and Price of N-[(4-methylphenyl)-sulfonyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl diphenylphosphinate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-[(4-methylphenyl)-sulfonyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl diphenylphosphinate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-[(4-methylphenyl)-sulfonyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl diphenylphosphinate

There total 2 articles about N-[(4-methylphenyl)-sulfonyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl diphenylphosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 23438-55-3
1-(4-Methylbenzene)sulfonyl-2H-hexahydroazepin-2-one

: 1499-21-4
Diphenylphosphinic chloride

: 960059-42-1
N-[(4-methylphenyl)-sulfonyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl diphenylphosphinate

Guidance literature:: 1-(4-Methylbenzene)sulfonyl-2H-hexahydroazepin-2-one; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 1h;

Diphenylphosphinic chloride; In tetrahydrofuran; at -78 - 20 ℃; Further stages.;
DOI:10.1039/b708967h

Reference yield: 44.0%

: 23438-55-3
1-(4-Methylbenzene)sulfonyl-2H-hexahydroazepin-2-one

: 1499-21-4
Diphenylphosphinic chloride

: 960059-36-3
C₁₃H₁₅NO₂S

: 960059-42-1
N-[(4-methylphenyl)-sulfonyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl diphenylphosphinate

Guidance literature:: 1-(4-Methylbenzene)sulfonyl-2H-hexahydroazepin-2-one; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 2h;

Diphenylphosphinic chloride; In tetrahydrofuran; at -78 - 20 ℃; Further stages.;
DOI:10.1039/b708967h

Reference yield: 64.0%

: 960059-42-1
N-[(4-methylphenyl)-sulfonyl]-4,5,6,7-tetrahydro-1H-azepin-2-yl diphenylphosphinate

: 5720-05-8
4-methylphenylboronic acid

: 1097200-74-2
N-[(4-methylphenyl)sulfonyl]-2-(4'-methylphenyl)-4,5,6,7-tetrahydro-azepane

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate; In 1,2-dimethoxyethane; water; at 85 ℃; Inert atmosphere;
DOI:10.1055/s-0029-1217067