trifluoro-methanesulfonic acid 4,5-bis-[4-(dodecane-1-sulfonyl)-phenylethynyl]-2-methoxy-phenyl ester

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Chemical Name:trifluoro-methanesulfonic acid 4,5-bis-[4-(dodecane-1-sulfonyl)-phenylethynyl]-2-methoxy-phenyl ester
CAS No.:483343-84-6
Molecular Formula:C₄₈H₆₃F₃O₈S₃
Molecular Weight:921.217
Hs Code.:

Synonyms:trifluoro-methanesulfonic acid 4,5-bis-[4-(dodecane-1-sulfonyl)-phenylethynyl]-2-methoxy-phenyl ester

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Chemical Property of trifluoro-methanesulfonic acid 4,5-bis-[4-(dodecane-1-sulfonyl)-phenylethynyl]-2-methoxy-phenyl ester

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Technology Process of trifluoro-methanesulfonic acid 4,5-bis-[4-(dodecane-1-sulfonyl)-phenylethynyl]-2-methoxy-phenyl ester

There total 7 articles about trifluoro-methanesulfonic acid 4,5-bis-[4-(dodecane-1-sulfonyl)-phenylethynyl]-2-methoxy-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 179925-11-2
1-(Dodecane-1-sulfonyl)-4-ethynyl-benzene

: 483343-80-2
4,5-diiodo-2-methoxyphenol triflate

: 483343-84-6
trifluoro-methanesulfonic acid 4,5-bis-[4-(dodecane-1-sulfonyl)-phenylethynyl]-2-methoxy-phenyl ester

Guidance literature:: With triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(02)01902-0

Reference yield:

: 106-53-6
para-bromobenzenethiol

: 483343-84-6
trifluoro-methanesulfonic acid 4,5-bis-[4-(dodecane-1-sulfonyl)-phenylethynyl]-2-methoxy-phenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / NaOH

2: 88 percent / H₂O₂ / acetic acid

3: NEt₃ / Pd(PPh₃)2Cl₂; CuI

4: Bu₄NF / tetrahydrofuran

5: 91 percent / NEt₃ / Pd(PPh₃)2Cl₂; CuI / dimethylformamide

With sodium hydroxide; tetrabutyl ammonium fluoride; dihydrogen peroxide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; acetic acid; N,N-dimethyl-formamide; 3: Sonogashira coupling / 5: Sonogashira coupling;
DOI:10.1016/S0040-4039(02)01902-0

Reference yield:

: 143-15-7
1-dodecylbromide

: 483343-84-6
trifluoro-methanesulfonic acid 4,5-bis-[4-(dodecane-1-sulfonyl)-phenylethynyl]-2-methoxy-phenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / NaOH

2: 88 percent / H₂O₂ / acetic acid

3: NEt₃ / Pd(PPh₃)2Cl₂; CuI

4: Bu₄NF / tetrahydrofuran

5: 91 percent / NEt₃ / Pd(PPh₃)2Cl₂; CuI / dimethylformamide

With sodium hydroxide; tetrabutyl ammonium fluoride; dihydrogen peroxide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; acetic acid; N,N-dimethyl-formamide; 3: Sonogashira coupling / 5: Sonogashira coupling;
DOI:10.1016/S0040-4039(02)01902-0