2-Methyl-5-((1S,2S,4R)-2-methyl-3-methylenebicyclo[2.2.1]heptan-2-yl)pent-2-en-1-ol

Base Information

Chemical Name:2-Methyl-5-((1S,2S,4R)-2-methyl-3-methylenebicyclo[2.2.1]heptan-2-yl)pent-2-en-1-ol
CAS No.:73890-74-1
Molecular Formula:C₁₅H₂₄O
Molecular Weight:220.355
Hs Code.:
European Community (EC) Number:234-262-4
DSSTox Substance ID:DTXSID601121647

Synonyms:santalol

Suppliers and Price of 2-Methyl-5-((1S,2S,4R)-2-methyl-3-methylenebicyclo[2.2.1]heptan-2-yl)pent-2-en-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-Methyl-5-((1S,2S,4R)-2-methyl-3-methylenebicyclo[2.2.1]heptan-2-yl)pent-2-en-1-ol

Chemical Property:

XLogP3:4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:220.182715385
Heavy Atom Count:16
Complexity:315

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=CCCC1(C2CCC(C2)C1=C)C)CO
Isomeric SMILES:C/C(=C\CC[C@]1([C@H]2CC[C@H](C2)C1=C)C)/CO

Technology Process of 2-Methyl-5-((1S,2S,4R)-2-methyl-3-methylenebicyclo[2.2.1]heptan-2-yl)pent-2-en-1-ol

There total 28 articles about 2-Methyl-5-((1S,2S,4R)-2-methyl-3-methylenebicyclo[2.2.1]heptan-2-yl)pent-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77-42-9,27542-07-0,27542-08-1,37172-32-0,42495-69-2,73890-74-1,77983-61-0,79081-89-3,79081-90-6,81893-42-7,98718-53-7,98718-54-8,130930-05-1,131726-06-2,131726-07-3
santalol

Guidance literature:: X, Lithiumaluminiumhydrid;
DOI:10.1016/S0040-4039(01)87560-2

Reference yield:

: 81967-89-7
β-santalene

: 77-42-9,27542-07-0,27542-08-1,37172-32-0,42495-69-2,73890-74-1,77983-61-0,79081-89-3,79081-90-6,81893-42-7,98718-53-7,98718-54-8,130930-05-1,131726-06-2,131726-07-3
rac-(Z)-β-santalol

Guidance literature:: β-santalene; With selenium(IV) oxide; In ethanol; for 4h; Heating;

With sodium tetrahydroborate; at 20 ℃;
DOI:10.1055/s-2005-864825

Reference yield:

: Dimethyl-[3-methyl-3-(4-methyl-pent-3-enyl)-bicyclo[2.2.1]hept-(2Z)-ylidenemethyl]-phenyl-silane

: 77-42-9,27542-07-0,27542-08-1,37172-32-0,42495-69-2,73890-74-1,77983-61-0,79081-89-3,79081-90-6,81893-42-7,98718-53-7,98718-54-8,130930-05-1,131726-06-2,131726-07-3
rac-(Z)-β-santalol

Guidance literature:: Multi-step reaction with 2 steps

1.1: 100 percent / HI / 5 h / Heating

2.1: SeO₂ / ethanol / 4 h / Heating

2.2: 68 mg / NaBH₄ / 20 °C

With selenium(IV) oxide; hydrogen iodide; In ethanol;
DOI:10.1055/s-2005-864825