<3--16-<(tetrahydro-2H-pyran-2-yl)oxy>hexadecanamide>propyl>carbamic acid, dibenzyl ester

Base Information

• Chemical Name: <3--16-<(tetrahydro-2H-pyran-2-yl)oxy>hexadecanamide>propyl>carbamic acid, dibenzyl ester
• CAS No.: 171019-90-2
• Molecular Formula: C₄₄H₆₉N₃O₇
• Molecular Weight: 752.048

Synonyms:<3--16-<(tetrahydro-2H-pyran-2-yl)oxy>hexadecanamide>propyl>carbamic acid, dibenzyl ester

Chemical Property of <3--16-<(tetrahydro-2H-pyran-2-yl)oxy>hexadecanamide>propyl>carbamic acid, dibenzyl ester

Chemical Property:

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Technology Process of <3--16-<(tetrahydro-2H-pyran-2-yl)oxy>hexadecanamide>propyl>carbamic acid, dibenzyl ester

There total 4 articles about <3--16-<(tetrahydro-2H-pyran-2-yl)oxy>hexadecanamide>propyl>carbamic acid, dibenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

<3-<<4-(carboxyamino)butyl>amino>propyl>carbamic acid, dibenzyl ester (89965-56-0) + 16-<(tetrahydro-2H-pyran-2-yl)oxy>hexadecanoic acid (171019-89-9) → <3--16-<(tetrahydro-2H-pyran-2-yl)oxy>hexadecanamide>propyl>carbamic acid, dibenzyl ester (171019-90-2)

Guidance literature:

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; for 27h; Ambient temperature;

DOI:10.1016/0040-4020(95)00697-7

Reference yield:

N-(3-aminopropyl)-1,4-diaminobutane (124-20-9) → <3--16-<(tetrahydro-2H-pyran-2-yl)oxy>hexadecanamide>propyl>carbamic acid, dibenzyl ester (171019-90-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 52 percent / CH₂Cl₂ / 3 h / Ambient temperature

2: 95 percent / dicyclohexylcarbodiimide, 1-hydroxybenzotriazole / tetrahydrofuran / 27 h / Ambient temperature

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;

DOI:10.1016/0040-4020(95)00697-7

Reference yield:

3-benzyloxycarbonyl-1,3-thiazolidine-2-thione (74058-68-7) → <3--16-<(tetrahydro-2H-pyran-2-yl)oxy>hexadecanamide>propyl>carbamic acid, dibenzyl ester (171019-90-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 52 percent / CH₂Cl₂ / 3 h / Ambient temperature

2: 95 percent / dicyclohexylcarbodiimide, 1-hydroxybenzotriazole / tetrahydrofuran / 27 h / Ambient temperature

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;

DOI:10.1016/0040-4020(95)00697-7

upstream raw materials:

<3-<<4-(carboxyamino)butyl>amino>propyl>carbamic acid, dibenzyl ester

16-<(tetrahydro-2H-pyran-2-yl)oxy>hexadecanoic acid

N-(3-aminopropyl)-1,4-diaminobutane

3-benzyloxycarbonyl-1,3-thiazolidine-2-thione

Downstream raw materials:

<3--16-hydroxyhexadecanamide>propyl>carbamic acid, dibenzyl ester

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